食品科学 ›› 2023, Vol. 44 ›› Issue (11): 167-176.doi: 10.7506/spkx1002-6630-20220426-331

• 包装贮运 • 上一篇    

百里香酚微胶囊的制备及其对草莓的保鲜效果

钟秋夏,郑海英,朱燕丽,李 晶,陈汉城,范小平   

  1. (1.华南农业大学食品学院,广东 广州 510642;2.广州市领航食品有限公司,广东 广州 510800;3.广东安德力新材料有限公司,广东 汕头 515824)
  • 发布日期:2023-06-30
  • 基金资助:
    2021年广东省科技专项资金(“大任务+任务清单”)项目(210714116891352); 2020年广东省科技创新战略专项资金(省重点实验室)项目(2020B121202008)

Preparation of Thymol-Containing Microcapsules and Its Application in Strawberry Preservation

ZHONG Qiuxia, ZHENG Haiying, ZHU Yanli, LI Jing, CHEN Hancheng, FAN Xiaoping   

  1. (1. College of Food Science, South China Agricultural University, Guangzhou 510642, China; 2. Guangzhou Linghang Food Limited Company, Guangzhou 510800, China; 3. Guangdong Andeli New Material Co., Ltd., Shantou 515824, China)
  • Published:2023-06-30

摘要: 百里香酚作为一种抗氧化剂与广谱抗菌剂,因溶解性差、稳定性低和气味刺激性强等缺点限制了其在食品保鲜领域的应用。本实验以百里香酚为芯材,β-环糊精为壁材,采用饱和水溶液法制备百里香酚微胶囊,研究百里香酚微胶囊的缓释性能、抑菌能力、抗氧化能力,结合扫描电子显微镜、傅里叶变换红外光谱、热重分析对百里香酚微胶囊结构进行表征,并分析百里香酚微胶囊对草莓的保鲜效果。结果表明,百里香酚被成功包埋在β-环糊精中,且微胶囊热稳定性得到明显提升。微胶囊在360 min时达到最大累积释放率41.16%,当微胶囊用量为25 mg时,对大肠杆菌、金黄色葡萄球菌有最强抑菌效果,当微胶囊质量浓度为10 mg/mL时,对1,1-二苯基-2-三硝基苯肼自由基清除率高达81.40%。将制备的百里香酚微胶囊应用在草莓保鲜实验中,在贮藏至第10天时,与空白对照组相比,微胶囊组草莓的腐烂率、质量损失率分别降低了26.34%、19.63%,此外,百里香酚微胶囊能够减缓草莓硬度、可溶性固形物质量分数的下降,且微胶囊组草莓的外观、色泽、质地、风味都呈现更好的保鲜效果。综上,百里香酚微胶囊可延缓草莓的腐败变质,有效地保持草莓的品质,在常温下可延长草莓的货架期。

关键词: 百里香酚;微胶囊;缓释;抗菌;草莓保鲜

Abstract: As an antioxidant and broad-spectrum antibacterial agent, thymol has some disadvantages such as poor solubility, low stability and strong irritating odor, restricting its application in food preservation. In order to overcome these shortcomings, thymol-containing microcapsules were prepared by the saturated aqueous solution method using thymol as the core material and β-cyclodextrin as the wall material, and the sustained release performance, antibacterial and antioxidant capacity of the microcapsules were evaluated. Meanwhile, its structure was characterized by scanning electron microscopy (SEM), Fourier transform infrared (FTIR) spectroscopy and thermogravimetric (TG) analysis, and its efficacy in preserving strawberry quality was analyzed. The results showed that thymol was successfully embedded in β-cyclodextrin and the thermal stability of the microcapsules was significantly improved. The maximum cumulative amount of thymol released from the microcapsules was 41.16% after 360 min. When used at a dosage of 25 mg, the microcapsules had the strongest antibacterial effect on Escherichia coli and Staphylococcus aureus. At a concentration of 10 mg/mL, it scavenged 81.40% of 1,1-diphenyl-2-picrylhydrazyl (DPPH) radicals. The microcapsules reduced the decay incidence and loss rate by 26.34% and 19.63%, respectively on the 10th day of storage compared with the control group, slowed the decrease in hardness and soluble solids content (SSC), and better maintained the appearance, color, texture and flavor. Thymol-containing microcapsules could delay the spoilage, effectively maintain the quality, and prolong the shelf life of strawberry at room temperature.

Key words: thymol; microcapsule; sustained release; antibacterial; strawberry preservation

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