Optimization of Extraction Process for Free Anthraquinone from Semen Cassiae by Response Surface Methodology

doi:10.7506/spkx1002-6630-201116040

FOOD SCIENCE ›› 2011, Vol. 32 ›› Issue (16): 192-195.doi: 10.7506/spkx1002-6630-201116040

• Processing Technology • Previous Articles Next Articles

Optimization of Extraction Process for Free Anthraquinone from Semen Cassiae by Response Surface Methodology

LI Jia1，WU Zhao-xia1,*，ZHANG Xuan1，ZHANG Qi1，XU Ya-ping2

(1. College of Food Science, Shenyang Agricultural University, Shenyang 110866, China； 2. Chaoyang Engineering Technical School, Chaoyang 122000, China)

Received:2018-05-21 Revised:2018-05-21 Online:2011-08-25 Published:2011-07-26

Abstract

Abstract: Anthraquinone is one of the major functional components in Cassia obtusifolia L. seeds. Response surface methodology was employed to optimize the ultrasonic-assisted extraction of free anthraquinone from Semen Cassiae. The extraction efficiency of free anthraquinone was investigated with respect to four process conditions including ethanol concentration, extraction temperature, ultrasonic treatment time and material-to-liquid ratio. The optimal conditions for anthraquinone extraction were 80% aqueous ethanol as the extraction solvent, material-to-liquid ratio of 15:1 (mL/g), extraction temperature of 65 ℃, ultrasonic treatment time of 30 min and ultrasonic power of 100 W. Under the optimal extraction conditions, the extraction rate of free anthraquinone from Semen Cassiae. was 28.32%.

Key words: Cassia obtusifolia L., ultrasonic, anthraquinone, response surface methodology

CLC Number:

TS201.2

LI Jia，WU Zhao-xia，ZHANG Xuan，ZHANG Qi，XU Ya-ping. Optimization of Extraction Process for Free Anthraquinone from Semen Cassiae by Response Surface Methodology[J]. FOOD SCIENCE, 2011, 32(16): 192-195.

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Optimization of Extraction Process for Free Anthraquinone from Semen Cassiae by Response Surface Methodology

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