FOOD SCIENCE ›› 2012, Vol. 33 ›› Issue (12): 149-153.doi: 10.7506/spkx1002-6630-201212029

• Analysis & Detection • Previous Articles     Next Articles

Solid Phase Microextraction and GC-MS Analysis of the Effect of Cumin Powder on Volatile Compounds in Low Sugar Cookies with Stevioside

ZHONG Jing1,WU Chao1,ABDEL-SAMIE Mohamed ABDEL-SHAFI1,WANG Feng1, HUANG Wei-ning1,*,ZHENG Jian-xian2   

  1. (1. State Key Laboratory of Food Science and Technology, Jiangnan University, Wuxi 214122, China; 2. School of Food and Bioengineering, South China University of Technology, Guangzhou 510640, China)
  • Online:2012-06-25 Published:2012-07-27

Abstract: In order to explore the effect of cumin power on volatile flavor compounds in low sugar cookies with stevioside, solid phase micro-extraction and gas chromatography-mass spectrometry were used to characterize the categories and contents of volatile flavor compounds in different cookie food systems, including normal cookies (control), low sugar cookies with 45% (m/m) sugar replaced by stevioside (S) and low sugar cookies with 10% (m/m) cumin powder (S+C). A total of 97 components were identified, and 16 of them were detected in all three samples, while 34 components were detected in low sugar cookies with stevioside (S) but not in the control. Meanwhile, only 25 components were observed in S+C. Aldehydes, ketones and esters were the major volatile compounds in the control samples, and heterocyclic compounds were significantly increased in S cookie samples with the addition of stevioside. The addition of cumin powder resulted in an obvious increase in the contents of aldehydes and alkenes in low-sugar cookies, which reached 48% and 26.51% (accounting for the total flavor compounds), respectively. The main aldehydes were cuminaldehyde (27.45%), 2-caren-10-al (15.01%) and phellandral (3.08%), and the main alkenes were α-pinene (8.08%), γ-terpinene (8.07%), limonene (1.91%) and β-myrcene (1.67%).

Key words: cookies, cumin, low sugar, stevioside, volatile compounds, solid phase micro-extraction/gas chromatography-mass spectrometry

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