[1] 韦异, 栗晖, 张英等. 柱色谱分离提纯三氯蔗糖[J]. 食品科学, 2002, 29(5): 87-89.[2] 李鹏飞, 李宗石, 乔卫红. 非营养型甜味剂—三氯蔗糖[J]. 化工进展, 2005, 24(11): 1253-1256.[3] MUFTI K S, KHAN R A. Process for the preparation of 4,1′,6′-trichloro-4,1′,6′-trideoxy galactose sucrose(TGS):US: 4380476 [P].1983-4-19.[4] HOUGH L, PHADNIS S P, TARELLI E. The preparation of 4,6-dichloro-4,6-deoxy-6′-chlorodeoxy -β-D-galactose sucrose and the conversion of chlorinated derivation into anhydrides[J]. Carbohydr Res, 1975, 44(1): 37-44.[5] 郑建仙, 李璇, 袁尔东. 全基团保护法制备三氯蔗糖的研究[J]. 食品与发酵工业, 2002, 33(2): 1-6.[6] NAVIA J L. Process for synthesizing sucrose derivatives by regioselective reaction: US: 4950746 [P]. 1990-08-21.[7] 马志玲, 王延平, 彭志英. 单酯法合成高甜度甜味剂—三氯蔗糖的研究[J]. 食品科学, 2002, 23 (5): 51-54.[8] CLARK J D, LEMAYR R R. Method for the synthesis of sucrose-6-esters: US: 6939962 [P]. 2005-09-6.[9] 陈金娥. 超级甜味剂三氯蔗糖的开发与研究[J]. 酿酒科技, 2007, 28(2): 29-34.[10] KHAN R A, SANKEY G H, SIMPSON P J. Chlorination of sugars: US: 5136031 [P]. 1992-08-4.[11] JONES J D,HACKING A J,CHEETHAM P J. Biological method for protection of 6-position of sucrose and its use in synthesis of disaccharide high-intensity sweeter[J]. Biotech&Bioeng. 1992. 39(2): 203-210.[12] BENNETT C,DORDICK J S,HACKING A J, et al. Biocatalytic synthesis of disaccharide high-intensity sweeterner sucralose via a tetrachlororaffinose intermediate[J]. Biotech&Bioeng, 1992, 39(2): 211-217.[13] CLARK J D, et al. An improved method for the synthesis of sucrose-6-esters: EP: 1305326 [P]. 2003-05-2.[14] WALKUP R E, NAVIA J L, et al. Sucrose-6-ester chlorination: US: 4980463 [P]. 1990-11-25.[15] 陆正清. 三氯蔗糖合成工艺研究[D]. 南京: 东南大学, 2006.[16] QUENEAU Y, FITREMANN J, TROMBOTTO S. The chemistry of unprotected sucrose:the selectivity issue[J]. C.R.Chimie, 2004, 7(2): 177-188.[17] 李晔, 晏日安, 李晓光, 等. 三氯蔗糖的基团迁移法合成研究[J]. 食品科学, 2004, 25(1): 50-52.[18] 陆正清. 蔗糖-6-乙酸酯氯化工艺的研究[J]. 食品科技, 2007, (3): 158-161.[19] 张建军. N-N二甲基甲酰胺与甲苯相互作用的1H NMR研究[J]. 河北师范大学学报(自然科学版), 1993, 1: 41-44.[20] 李松林, 周亚平, 刘俊吉. 物理化学(下册)[M]. 第五版. 北京: 高等教育出版社, 2009: 542-543. |