FOOD SCIENCE ›› 2023, Vol. 44 ›› Issue (14): 326-335.doi: 10.7506/spkx1002-6630-20220905-046

• Component Analysis • Previous Articles     Next Articles

Analysis of Major Aroma Compounds in Fermented and Prepared Hawthorn Wine

GU Peishan, CHEN Yixin, WANG Chunguang, ZHU Yuxuan, CHANG Xiaomin, WANG Sisi, ZHU Baoqing, WANG Houyin   

  1. (1. Beijing Key Laboratory of Forestry Food Processing and Safety, College of Biological Sciences and Technology, Beijing Forestry University, Beijing 100083, China; 2. Food and Agriculture Standardization Institute, China National Institute of Standardization, Beijing 100191, China)
  • Online:2023-07-25 Published:2023-08-11

Abstract: In this study, liquid-liquid extraction-solvent assisted flavor evaporation (LLE-SAFE), headspace solid phase microextraction extraction (HS-SPME), gas chromatography-quadrupole-mass spectrometry (GC-Quadrupole-MS), gas chromatography-orbitrap-mass spectrometry (GC-Orbitrap-MS) and gas chromatography-olfactometry (GC-O) were used in combination to identify the volatile components in a fermented hawthorn wine (SBL-J) and a prepared hawthorn wine (FS), and the results of sensory analysis, modified frequency (MF) and odor activity value (OAV) were used to determine the key aroma compounds. Totally 89 aroma compounds were identified by LLE-SAFE/GC-O-MS. In addition, 29 and 38 aroma compounds with MF values of more than 20% were found in SBL-J and FS, respectively. A total of 123 volatile components were detected by HS-SPME/GC-Quadrupole-MS and HS-SPME/GC-Orbitrap-MS and there were 29 and 33 aroma compounds with OAV of greater than 1 (0.1 for esters) identified in SBL-J and FS, respectively. 2-Methybutyl acetate, ethyl hexanoate, ethyl octanoate and phenylethyl alcohol were the key aroma compounds in the two samples. To our knowledge, 2-methybutyl acetate, ethyl isovalerate, (E,E)-2,4-hexadienoic acid ethyl ester and ethyl butyrate, were identified for the first time as the key aroma components of hawthorn wine.

Key words: hawthorn wine; gas chromatography-mass spectrometry-olfactometry; gas chromatography-orbitrap-mass spectrometry; odor activity value; aroma compounds

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