FOOD SCIENCE ›› 2002, Vol. 23 ›› Issue (2): 108-110.

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Simultaneous Determination of Harm ful Elements Pb,Cd,Cr,Hg,As and Se i n Freshwater Products with Microwave Digestion by ICP -AES

 XIE  Hua-Lin   

  • Online:2002-02-15 Published:2012-02-13

Abstract: The paper developed a newmethod of mi crowave sample degestion by ICP -AES to simultanuously deter-mine Pb,Cd,Cr,Hg,As and Se.Under th e optimumconditions,the detection limits of Pb,Cd,Cr,Hg and As were0.0008,0.0007,0.0018,0.0028,0.0012,0.0046μg /Lrespectively.The recoveries of the methodwere94.5%~104.2%,and RSD1.4%~2.6%.This method was accurate,quickly -accessible andconvenient.It was used in the determination of freshwater with th e result satisfactory.

Key words: Microwave digestionof samples , ICP –AES, Freshwater , Pb , Cd , Cr , Hg , As , Se