Study on High Performance Liquid Chromatography Fingerprint of Shixia Longan

doi:10.7506/spkx1002-6630-200904030

FOOD SCIENCE ›› 2009, Vol. 30 ›› Issue (4): 154-157.doi: 10.7506/spkx1002-6630-200904030

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Study on High Performance Liquid Chromatography Fingerprint of Shixia Longan

XIAO Wei-qiang，DAI Hong-fen，HUANG Bing-xiong，LI Jian-guang，LIU Chuan-he，WANG Xiao-rong*

(Institute of Pomology, Guangdong Academy of Agricultural Sciences, Guangzhou 510640, China)

Received:2008-02-15 Revised:2008-07-11 Online:2009-02-15 Published:2010-12-29
Contact: XIAO Wei-qiang E-mail:xwq6817@126.com

Abstract

Abstract:

In this study, HPLC analysis on Shixia longan (Dimocarpus longan Lour. cv. Shixia) was performed on reversedphase Nucleosil C18 column (250 mm × 4.0 mm, 5 μm) by using mobile phase 0.01 mol/L KH2PO4 and CH3OH, dual gradient elution was proceeded with the flow rate of 0.8 ml/min, and operation conditions were set as follows: detection at 260 nm and column temperature 40 ℃. Results showed that there are 13 common peaks in HPLC chromatogram of water-soluble components of 14 Shixia longan samples collected from different areas. Moreover, by calculated with fingerprint analysis system of Chinese medicine, relative standard deviations (RSD) of relative retained time of common peaks are below 1.2% and their similarity is above 0.967. Therefore, the established chromatographic fingerprint is proved to be a scientific quality evaluation method for Shixia longan.

Key words: HPLC, Dimocarpus longan Lour. cv. Shixia, nucleoside, fingerprint

CLC Number:

R151.3

XIAO Wei-qiang，DAI Hong-fen，HUANG Bing-xiong，LI Jian-guang，LIU Chuan-he，WANG Xiao-rong*. Study on High Performance Liquid Chromatography Fingerprint of Shixia Longan[J]. FOOD SCIENCE, 2009, 30(4): 154-157.

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Study on High Performance Liquid Chromatography Fingerprint of Shixia Longan

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