Comparative Analysis of Volatile Components of Vanilla Grown in Hainan by Solid Phase Micro-Extraction and Simultaneous Distillation Extraction

doi:10.7506/spkx1002-6630-201402029

FOOD SCIENCE

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Comparative Analysis of Volatile Components of Vanilla Grown in Hainan by Solid Phase Micro-Extraction and Simultaneous Distillation Extraction

DONG Zhi-zhe1,2, GU Feng-lin2,3, XU Fei2,3, WANG Qing-huang2,3,*

1. College of Food Science and Technology, Huazhong Agricultural University, Wuhan 430070, China;
2. Spice and Beverage Research Institute, Chinese Academy of Tropical Agricultural Sciences, Wanning 571533, China;
3. Key Laboratory of Genetic Resources Utilization of Spice and Beverage Crops, Ministry of Agriculture, Wanning 571533, China

Online:2014-01-25 Published:2014-02-19
Contact: WANG Qing-huang

Abstract

Abstract:

The conditions of solid phase micro-extraction (SPME) for extraction of volatile components in vanilla grown in
Hainan were optimized and its effectiveness was compared with that of simultaneous distillation extraction (SDE) for the
analysis of volatile components in vanilla by gas chromatography coupled with mass spectrometry (GC-MS). The results
showed the optimal SPME conditions were established using a 75 μm carboxen®/polydimethylsiloxane (CAR/PDMS) fiber
at 80 ℃ for 20 min. A total of 105 volatile components were identified, among which, 73 volatile compounds were extracted
by SDE and 78 by SPME. This study has shown that more volatile components can be extracted and identified with a
combination of SPME and SDE.

Key words: vanilla, solid phase micro-extraction, simultaneous distillation extraction, optimization

CLC Number:

TQ651

DONG Zhi-zhe1,2, GU Feng-lin2,3, XU Fei2,3, WANG Qing-huang2,3,*. Comparative Analysis of Volatile Components of Vanilla Grown in Hainan by Solid Phase Micro-Extraction and Simultaneous Distillation Extraction[J]. FOOD SCIENCE, doi: 10.7506/spkx1002-6630-201402029.

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Comparative Analysis of Volatile Components of Vanilla Grown in Hainan by Solid Phase Micro-Extraction and Simultaneous Distillation Extraction

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