食品科学 ›› 2010, Vol. 31 ›› Issue (2): 220-223.doi: 10.7506/spkx1002-6300-201002056

• 分析检测 • 上一篇    下一篇

紫花芒果实香气成分的GC-MS 分析

魏长宾,邢姗姗,刘胜辉,武红霞,王松标,臧小平,马蔚红*   

  1. 中国热带农业科学院南亚热带作物研究所
  • 收稿日期:2009-03-25 修回日期:2009-08-10 出版日期:2010-01-15 发布日期:2010-12-29
  • 通讯作者: 马蔚红 E-mail:zjwhma@163.com
  • 基金资助:

    农业部“948”项目(2006G33);中央级公益性科研院所基本科研业务费专项;
    国家林业局林业科技支撑计划项目(2006BAD01A1705);农业部公益性行业(农业)科研专项(nyhyzx07-032-3)

GC-MS Analysis of Volatile Components of Mango (Mangifera indica L. var Zihua) Fruits

WEI Chang-bin,XING Shan-shan,LIU Sheng-hui,WU Hong-xia,WANG Song-biao,
ZANG Xiao-ping,MA Wei-hong*   

  1. (South Subtropical Crops Research Institute, Chinese Academy of Tropical Agricultural Sciences, Zhanjiang 524091, China)
  • Received:2009-03-25 Revised:2009-08-10 Online:2010-01-15 Published:2010-12-29
  • Contact: MA Wei-hong* E-mail:zjwhma@163.com

摘要:

使用75μm Carboxen/PDMS 和100μm 聚二甲基硅氧烷(polydimethylsiloxane,PDMS)两种萃取头提取紫花芒果成熟时果肉和果皮的香气成分,并用气质联用仪定性定量分析香气成分。使用75μm CAR/PDMS 萃取头检出果皮香气成分26 种,占总挥发物的98.71%,萜类成分占98.49%,挥发性成分相对含量较高的是萜品油烯(44.20%);果肉香气检出21 种挥发物,占总挥发物的99.29%,其中萜类占97.82%,相对含量较高的是对伞花烃(55.45%)。使用100μm PDMS 萃取头检出果皮香气中22 种挥发物,占总挥发物的98.51%,萜类成分占98.14%,其中相对含量较高的是萜品油烯(68.45%);果肉香气中检出15 种挥发性成分,占总挥发物的97.68%,萜类占96.69%,相对含量较高的是萜品油烯(79.18%)。紫花芒果更适合使用75μm Carboxen/PDMS 提取香气成分进行分析,且果皮中的香气成分多于果肉中,主要是萜类成分。

关键词: 芒果, 萃取头, 香气, 气相色谱- 质谱联用

Abstract:

The volatile components in ripening fruit peel and pulp of mango (Mangifera indica L. var Zihua) were extracted with 100 μm PDMS or 75 μm Carboxen/ PDMS fibres prior to GC-MS analysis. Twenty-six volatile components were identified in mango peel extracted with 75μm Carboxen/ PDMS fibre, accounting for 98.71% of total volatile components. Terpenes contributed to 98.49% of identified components, among which terpinolene constituted a major fraction, accounting for 44.20%. Totally 21 components were detected in mango pulp, occupying 99.29% of total volatile components. Terpenes made a contribution of 97.82%, in which p-cymene was a dominant compound (55.45%). However, only 22 volatile components were identified in mango peel extracted with 100 μm PDMS fibre, which accounted for 98.51% of total volatile components, comprising 98.14% of terpenes and the content of terpinolene was 68.45%. Fifteen volatile components were found in mango pulp, the total relative content 97.68%, and the content of terpenes 96.69% with the dominant terpinolene of 79.18%. Therefore, 75 μm Carboxen/ PDMS fibre provides a much more suitable tool for the extraction of volatile components in mango fruits and the peel seems to contain more volatile components than the pulp in quantity, and the main volatile is terpenes.

Key words: mango, solid-phase microextraction (SPME) fibre, volatile aroma, gas chromatography-mass spectrometry (GC-MS)

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