食品科学 ›› 2010, Vol. 31 ›› Issue (12): 119-122.doi: 10.7506/spkx1002-6630-201012027

• 工艺技术 • 上一篇    下一篇

超声波液态CO2提取分离芹菜籽油工艺条件优化的研究

徐华民   

  1. 哈尔滨工业大学分离技术中心
  • 收稿日期:2009-09-23 出版日期:2010-06-15 发布日期:2010-12-29
  • 通讯作者: 徐华民 E-mail:xuhuamin871130@sina.com

Ultrasonic-assisted Liquid Carbon Dioxide Extraction of Celery Seed Oil

XU Hua-min   

  1. Separation Technology Center, Harbin Institute of Technology, Harbin 150001, China
  • Received:2009-09-23 Online:2010-06-15 Published:2010-12-29
  • Contact: XU Hua-min E-mail:xuhuamin871130@sina.com

摘要:

目的:优选超声波液态CO2 提取分离芹菜籽油的工艺条件。方法:通过单因素试验和正交试验考察提取压力、超声时间、超声功率和料液比对芹菜籽油得率的影响。结果:以液态CO2 提取芹菜籽油各因素对芹菜籽油得率的影响大小依次为超声时间>超声功率>提取压力>料液比,优化的提取工艺参数为超声时间30min、超声功率100W、提取压力4MPa、料液比1:7(m/V),在此操作条件下,芹菜籽油得率2.8%。结论:超声波液态CO2提取分离芹菜籽油是一种有效的新型分离技术。

关键词: 芹菜籽油, 超声波提取, 液态CO2, 工艺优化

Abstract:

Objective: To optimize the extraction of celery seed oil with liquid carbon dioxide under the assistance of ultrasonic for achieving maximum oil yield. Methods: The effects of four process conditions, i.e., extraction pressure, length of extraction time, ultrasonic power and material-to-liquid ratio on the yield of celery seed oil were investigated using single factor and orthogonal array design methods. Results: The significance sequence of the conditions influencing the yield of celery seed oil was as follows: length of extraction time > ultrasonic power > extraction pressure > material-to-liquid ratio, and their optimum values were as follows: temperature 30 min, ultrasonic power 100 W, extraction pressure 4 MPa and material-to-liquid ratio 1:7 (m/V). Under these conditions, the yield of celery seed oil reached up to 2.8%. Conclusion: Ultrasonic-assisted liquid carbon dioxide extraction provides a new and efficient separation technique for celery seed oil extraction.

Key words: celery seed oil, ultrasonicd-assisted extraction, liquid carbon dioxide, orthogonal array design

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