食品科学 ›› 2010, Vol. 31 ›› Issue (20): 256-259.doi: 10.7506/spkx1002-6630-201020051

• 工艺技术 • 上一篇    下一篇

醇提超临界蜂胶剩余物的性质及其微胶囊粉末的制备

吉 挺,李文艳,岑 宁,吴宏安   

  1. 扬州大学动物科学与技术学院
  • 收稿日期:2009-09-27 修回日期:2010-09-27 出版日期:2010-10-25 发布日期:2010-12-29
  • 通讯作者: 吉挺 E-mail:jiting12@sohu.com
  • 基金资助:

    国家现代农业(蜂)产业技术体系项目(nycytx-43-5yz5);江苏省科技攻关项目(BE2007321)

Characterization and Microencapsulation of Alcohol Extract from Propolis Residue Left after SFE-CO2 Extraction

JI Ting,LI Wen-yan,CEN Ning,WU Hong-an   

  1. College of Animal Science and Technology, Yangzhou University, Yangzhou 225009, China
  • Received:2009-09-27 Revised:2010-09-27 Online:2010-10-25 Published:2010-12-29
  • Contact: JI Ting E-mail:jiting12@sohu.com

摘要:

对超临界蜂胶的利用价值及其应用进行探讨。采用HPLC 法、国家标准法对蜂胶黄酮种类、总黄酮含量和抗氧化能力进行测定,采用冷冻干燥法对剩余物进行包埋。结果表明:醇提超临界萃取蜂胶剩余物的总黄酮含量为118.798mg/kg,与醇提蜂胶接近;不同蜂胶品对油脂的过氧化保护作用的强弱顺序是醇提蜂胶>醇提超临界萃取蜂胶剩余物>超临界蜂胶,说明超临界蜂胶剩余物也有一定的抗氧化作用;包埋后制备出的微胶囊产品粉质细腻、质地疏松,包埋率可达到69.87%。

关键词: 蜂胶, 再利用, 总黄酮, 抗氧化, 微胶囊

Abstract:

In order to elevate the utilization value of propolis residue from supercritical carbon dioxide fluid (SFE-CO2) extraction, the residue was reextracted with absolute alcohol, and the extract obtained was subjected to comparisons with alcohol and SFE-CO2 extracts from propolis for differences in flavonoid compound composition and antioxidant effect and to microencapsulation by lyophilization. Total flavonoid content in the alcohol extract from propolis residues left after SFE-CO2 extraction was 118.798 mg/kg, which was close to the alcohol extract from propolis. The protective effects of different propolis products on the peroxidation of lard were different and deceased in the following order: the alcohol extract from propolis> the alcohol extract from propolis residue left after SFE-CO2 extraction > the SFE-CO2 extract from propolis. Thus, the alcohol extract from propolis residue left after SFE-CO2 extraction is a superior antioxidant. Its microcapsules were exquisite powder with a loose texture and the embedding rate was 69.87%.

Key words: propolis, recycling, total flavonoids, antioxidation, microcapsule

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