食品科学 ›› 2014, Vol. 35 ›› Issue (6): 107-112.doi: 10.7506/spkx1002-6630-201406022

• 分析检测 • 上一篇    下一篇

气相色谱-质谱法分析比较不同酵母发酵红树莓果酒的香气成分

王家利1,辛秀兰2,陈 亮2,陶伯旭1,张 丹3,杨晓清1,*   

  1. 1.内蒙古农业大学食品科学与工程学院,内蒙古 呼和浩特 010018;2.北京电子科技职业学院生物工程学院,
    北京 100029;3.西部钻探克拉玛依钻井公司,新疆 克拉玛依 834000
  • 收稿日期:2013-01-08 修回日期:2014-02-01 出版日期:2014-03-25 发布日期:2014-04-04
  • 通讯作者: 杨晓清 E-mail:yxqnmg@yahoo.com.cn
  • 基金资助:

    公益性行业(农业)科研专项(201103037);北京市属高等学校人才强教深化计划项目(nyhyzx07-028);
    科研基地-生物技术在制药和农产品加工中的应用平台建设项目(PXM2010_014306_109857)

Comparative Analysis by Gas Chromatography-Mass Spectrometry of Aromatic Composition of Red Raspberry Wines Fermented by Different Yeast Starters

WANG Jia-li1, XIN Xiu-lan2, CHEN Liang2, TAO Bo-xu1, ZHANG Dan3, YANG Xiao-qing1,*   

  1. 1. College of Food Science and Engineering, Inner Mongolia Agricultural University, Hohhot 010018, China;
    2. College of Bioengineering, Beijing Polytechnic, Beijing 100029, China;
    3. Karamay Drilling Company of Xibu Drilling Engingeering Company, Karamay 834000, China
  • Received:2013-01-08 Revised:2014-02-01 Online:2014-03-25 Published:2014-04-04
  • Contact: YANG Xiao-qing E-mail:yxqnmg@yahoo.com.cn

摘要:

以红树莓为原料,选取1203、1399、SY、RW、F151、F152 6 种果酒酵母进行发酵,通过顶空-固相微萃取法和气相色谱-质谱联用法分别对6 种果酒香气成分萃取、鉴定、分析和比较。结果表明:6 种酵母发酵的酒液中共检测出159 种香气成分,分别为45、56、67、58、66、39 种,其中相同成分占13 种。6 种果酒中的主要香气成分分别为乙醇、癸酸乙酯、辛酸乙酯、癸酸乙酯、癸酸乙酯、癸酸乙酯,含量依次为15.73%、22.05%、15.74%、18.38%、19.14%、15.24%。通过仪器测定和嗅闻感官综合判断,果酒酵母1399发酵的红树莓果酒香气较好,适宜大众口味。

关键词: 红树莓果酒, 顶空-固相微萃取法, 气相色谱-质谱联用, 香气成分

Abstract:

The aroma composition of red raspberry wines fermented by different wine yeast starters 1203, 1399, SY, RW,
F151 and F152 was analyzed and compared by headspace solid-phase microextraction (HS-SPME) and gas chromatographymass
spectrometry (GC-MS). In total 159 flavor components were detected in 6 red raspberry wines, with 45, 56, 67, 58, 66
and 39 ones in the corresponding individuals and 13 ones common to them. The main aroma components of the 6 wines were
alcohol, decanoic acid ethyl ester, octylic acid ethyl ester, decanoic acid ethyl ester, decanoic acid ethyl esterand decanoic
acid ethyl ester with contents of 15.73%, 22.05%, 15.74%, 18.38%, 19.14% and 15.24%, respectively. Through instrumental
analysis and sensory evaluation, it is concluded that raspberry wine fermented by wine yeast 1399 has an excellent aroma
and is suitable for the pubic taste.

Key words: red raspberry wine, headspace solid-phase microextraction (HS-SPME), gas chromatography-mass spectrometry (GC-MS), aroma components

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