食品科学 ›› 2022, Vol. 43 ›› Issue (8): 213-219.doi: 10.7506/spkx1002-6630-20210901-004

• 成分分析 • 上一篇    

4 种胡椒精油风味特征分析

段梦雅,王福清,吴桂苹,李鑫,谷风林,林毅,侯梅芳   

  1. (1.上海应用技术大学生态技术与工程学院,上海 201418;2.中国热带农业科学院香料饮料研究所,海南 万宁 571533;3.青藏高原特色农牧产品深加工国家地方联合工程研究中心,西藏 拉萨 850600;4.国家重要热带作物工程技术研究中心,海南 万宁 571533;5.海南省特色热带作物适宜性加工与品质控制重点实验室,海南 万宁 571533;6.华中农业大学食品科学技术学院,湖北 武汉 430070)
  • 发布日期:2022-04-26
  • 基金资助:
    “十三五”国家重点研发计划重点专项(2020YFD1001200)

Analysis of Flavor Characteristics of Four Pepper Essential Oils

DUAN Mengya, WANG Fuqing, WU Guiping, LI Xin, GU Fenglin, LIN Yi, HOU Meifang   

  1. (1. School of Ecological Technology and Engineering, Shanghai Institute of Technology, Shanghai 201418, China;2. Spice and Beverage Research Institute, Chinese Academy of Tropical Agricultural Sciences, Wanning 571533, China;3. National Joint Engineering Research Center for Intensive Processing of Special Agricultural and Animal Products in Tibetan Plateau, Lhasa 850600, China; 4. National Center of Important Tropical Crops Engineering and Technology Research, Wanning 571533, China; 5. Key Laboratory of Processing Suitability and Quality Control of the Special Tropical Crops of Hainan Province, Wanning 571533, China; 6. College of Food Science and Technology, Huazhong Agricultural University, Wuhan 430070, China)
  • Published:2022-04-26

摘要: 研究以黑胡椒、白胡椒、青胡椒和胡椒鲜果为原料提取的精油及精油风味特征。采用水蒸气蒸馏法提取精油,比较不同胡椒的精油提取得率,通过气相色谱-质谱法、电子鼻及定量描述性感官分析,对不同胡椒精油风味特征进行分析。结果表明,黑胡椒、白胡椒、青胡椒和胡椒鲜果的精油提取得率分别为1.718、1.867、1.487 mL/100 g和3.229 mL/100 g,胡椒鲜果的精油提取得率显著高于白胡椒、黑胡椒和青胡椒。从4 种胡椒精油中共鉴定出48 种物质,主要成分均为β-石竹烯、3-蒈烯、D-柠檬烯、β-蒎烯、δ-榄香烯、β-月桂烯。电子鼻数据证实,判别因子分析比主成分分析更易区分不同胡椒精油。感官评价显示胡椒鲜果精油的胡椒香比其他3 种精油明显,接受程度更高。偏最小二乘回归分析结果表明,芳香、草本、胡椒香属性与(+)-α-蒎烯成分呈正相关。实验结果为胡椒精油产品开发及升级提供参考。

关键词: 胡椒;精油;气相色谱-质谱法;风味;偏最小二乘回归分析

Abstract: The aim of this study is to explore the yield and flavor characteristics of essential oils extracted from black pepper, white pepper, green pepper, and fresh pepper fruit. The essential oils were extracted by steam distillation, and the extraction yields of different pepper essential oils were compared. The flavor characteristics of different pepper essential oils were analyzed by gas chromatography-mass spectrometry (GC-MS), electronic nose and quantitative descriptive sensory analysis. The results showed that the extraction yield of essential oil from fresh pepper fruit was 3.229 mL/100 g, which was significantly higher than that from white pepper, black pepper, and green pepper (1.718, 1.867, and 1.487 mL/100 g, respectively). A total of 48 volatile substances were identified from the four pepper essential oils, the main ones being β-caryophyllene, 3-carene, D-limonene, β-pinene, δ-elemene, and β-myrcene. The electronic nose data confirmed that discriminant function analysis (DFA) distinguished different pepper essential oils better than principal component analysis (PCA). The sensory evaluation showed that the pepper-like aroma of the essential oil of fresh pepper fruit was stronger than the other three essential oils and had higher acceptance. The results of partial least squares regression (PLSR) analysis showed that the aromatic?plant-like, herbal, and pepper-like aroma properties were positively correlated with (+)-α-pinene components. The experimental results provide a reference for the development and upgrading of pepper essential oil products.

Key words: pepper; essential oil; gas chromatography-mass spectrometry; flavor; partial least squares regression analysis

中图分类号: