食品科学 ›› 2007, Vol. 28 ›› Issue (9): 481-484.

• 分析检测 • 上一篇    下一篇

苍耳子风湿药酒的研制与检测

 戚颖欣, 曹柏营, 寇莹, 昌友权   

  1. 吉林工程技术师范学院生物与食品工程学院; 吉林工程技术师范学院生物与食品工程学院 吉林长春130052; 吉林长春130052;
  • 出版日期:2007-09-15 发布日期:2011-11-22

Development and Determination of Fengshi Medical Wine of Fructus xanthii

 QI  Ying-Xin, CAO  Bai-Ying, KOU  Ying, CHANG  You-Quan   

  1. College of Biology and Food Engineering,Jilin Teacher’s Institute of Engineering and Techology,Changchun 130052,China
  • Online:2007-09-15 Published:2011-11-22

摘要: 实验确定了回流提取法为苍耳子药酒生产的最佳工艺,建立苍耳子风湿药酒的质量标准,利用高效液相色谱法检测苍耳子有效成分绿原酸。绿原酸进样量在0.315~1.575μg范围内呈良好的线性关系,回归方程为Y=1857900X+7575.80,r=0.999985(n=5),平均加样回收率为99.22%,RSD值为1.38%(n=6)。结果表明本方法简便、快速、灵敏、准确、重复性好,可以控制苍耳子风湿药酒的质量。

关键词: 苍耳子, 风湿药酒, 高效液相色谱

Abstract: Experimentntal results inchicated that the optimal production method of Fengshi medical wine of Fructus xanthii was circumfluence extraction.An RP-HPLC method was established for determination of chloralgenic acid in Fengshi medical wine of Fructus xanthii.The calibration curve was in good linearity over the range of 0.315~1.575μg with the regression equation Y=1857900X+7575.80,r=0.999985(n=5).The average recovery was 99.22% with RSD=1.38%(n=6).The method appeared to be simple,accurate,reproducible and could be used to control the quality of Fengshi medical wine of Fructus xanthii.

Key words: Fructus xanthii, Fengshi medical wine, HPLC