食品科学 ›› 2009, Vol. 30 ›› Issue (24 ): 425-427.doi: 10.7506/spkx1002-6630-200924097

• 分析检测 • 上一篇    下一篇

两种不同粒度的马兰籽中脂肪酸的GC-MS 分析

姜显光,侯冬岩,回瑞华,李铁纯,刘晓媛,李秀铭   

  1. 鞍山师范学院化学系
  • 收稿日期:2009-07-29 出版日期:2009-12-15 发布日期:2010-12-29
  • 通讯作者: 姜显光, E-mail:happyjxg@tom.com
  • 基金资助:

    鞍山师范学院科研项目(09kyxm03)

Analysis of Fatty Acids in Kalimeris indica Seeds by Gas Chromatography-Mass Spectrometry

JIANG Xian-guang,HOU Dong-yan,HUI Rui-hua,LI Tie-chun,LIU Xiao-yuan,LI Xiu-ming   

  1. Department of Chemistry, Anshan Normal University, Anshan 114007, China
  • Received:2009-07-29 Online:2009-12-15 Published:2010-12-29
  • Contact: JIANG Xian-guang, E-mail:happyjxg@tom.com

摘要:

采用索氏提取法对两种不同粒度的马兰籽提取马兰籽油,进行甲酯化处理,以气相色谱- 质谱联用仪进行分析,对它们的脂肪酸组成和相对含量进行比较。结果表明:粒度大于1mm 和粒度小于1mm 分别鉴定出16 种和14 种脂肪酸,分别占马兰籽油总量的98.66% 和96.84%,两种不同粒度的马兰籽提出的马兰籽油中鉴定出主要脂肪酸均为十八碳二烯酸、十八碳烯酸、十六酸。

关键词: 马兰籽, 脂肪酸, 不同粒度, 索氏提取法, 气相色谱- 质谱联用仪

Abstract:

Kalimeris indica seed oil was extracted by Soxhlet extraction from Kalimeris indica seeds with two different granule sizes. Fatty acids in Kalimeris indica oil were esterified and analyzed by gas chromatography-mass spectrometry (GC-MS). Components and relative contents of fatty acids were compared. Results indicated that 16 fatty acids were identified in Kalimeris indica seeds with granule size larger than 1 mm and 14 fatty acids were identified in Kalimeris indica seeds with granule size less than 1 mm. Contents of total fatty acids were 98.66% and 96.84% in both kinds of Kalimeris indica seed oil, respectively. The major fatty acids in Kalimeris indica seeds were octadecadienoic acid, octadecenoic acid and hexadecanoic acid.

Key words: Kalimeris indica seed, fatty acid, granule size, Soxhlet extraction, gas chromatography-mass spectrometry (GC-MS)

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