食品科学 ›› 2024, Vol. 45 ›› Issue (8): 72-78.doi: 10.7506/spkx1002-6630-20230709-080

• 食品化学 • 上一篇    下一篇

山核桃分离蛋白为壁材的山核桃油微胶囊制备及其性能分析

李新,信钰,孙悦,齐斌,王立梅   

  1. (1.常熟理工学院生物与食品工程学院,苏州市食品生物技术重点实验室,江苏 常熟 215500;2.苏州大学药学院,江苏 苏州 215127)
  • 出版日期:2024-04-25 发布日期:2024-05-01
  • 基金资助:
    江苏省重点研发计划重点项目(BE2020386);江苏省政策引导类计划(苏北科技专项)(SZ-LYG202128)

Preparation and Performance Analysis of Manchurian Walnut Oil Microcapsules with Manchurian Walnut Protein Isolate as Wall Material

LI Xin, XIN Yu, SUN Yue, QI Bin, WANG Limei   

  1. (1. Suzhou Key Laboratory of Food Biotechnology, School of Biological and Food Engineering, Changshu Institute of Technology, Changshu 215500, China; 2. College of Pharmaceutical Sciences, Soochow University, Suzhou 215127, China)
  • Online:2024-04-25 Published:2024-05-01

摘要: 本实验以麦芽糊精、蛋黄粉、山核桃分离蛋白和大豆分离蛋白为微胶囊的壁材,通过不同比例的组合复配,采取喷雾干燥法制备山核桃油微胶囊产品,分析微胶囊的微观形貌、热稳定性、贮藏稳定性以及抗氧化稳定性,研究不同壁材组合得到的微胶囊的性能。结果显示,以山核桃分离蛋白为壁材制备的山核桃油微胶囊包埋率达到73.68%,微胶囊结构完整致密,成功将山核桃油芯材包埋在内部并具有保护芯材的作用。微胶囊粉末具备一定的流动性、溶解性好。山核桃分离蛋白微胶囊在程序升温条件下(10 ℃/min),低于150 ℃条件下质量损失仅为5.48%,远低于大豆分离蛋白微胶囊(10.3%),因此更能够满足大多数食品的热加工需要。微胶囊化明显减缓山核桃油氧化速度,提高了山核桃油的贮藏稳定性。抗氧化性实验证明山核桃油微胶囊能有效提高山核桃油中活性成分的抗氧化稳定性。通过评价山核桃分离蛋白这一新颖的微胶囊壁材的性能,发现山核桃分离蛋白是一种卓越的微胶囊壁材,扩大了蛋白质壁材的选择范围。同时,为核桃分离蛋白资源的应用提供新的思路,提高了山核桃的附加值。

关键词: 微胶囊;山核桃油;山核桃分离蛋白;壁材;包埋率

Abstract: Mixtures of maltodextrin (MD), egg yolk protein (EYP), Manchurian walnut protein isolate (MWPI) and soybean protein isolate (SPI) in different proportions were used as wall materials to prepare Manchurian walnut oil microcapsules by spray drying. The micromorphology, thermal stability, storage stability and antioxidant stability of microcapsules were analyzed. The results showed that the encapsulation efficiency of microcapsules prepared with MWPI was 73.68%, with an intact and dense structure, indicating that Manchurian walnut oil was successfully encapsulated in and protected by the microcapsules. The microcapsule powder had good flowability and solubility. The MWPI microcapsules lost only 5.48% of its initial mass under programmed heating conditions (10 ℃/min, up to 150 ℃), which was much lower than that of SPI microcapsules (10.3%), thereby being more able to meet the requirements of most thermally processed products. Microencapsulation obviously slowed down the oxidation rate of Manchurian walnut oil and improved its storage stability. The antioxidant experiments demonstrated that microencapsulation could effectively improve the antioxidant stability of active ingredients in Manchurian walnut oil. Therefore, this study demonstrated MWPI to be an excellent microcapsule wall material by evaluating its performance, which will expand the range of selection of protein-based wall materials, and provide a new idea for the application of walnut protein isolate resources to improve the added value of Manchurian walnut.

Key words: microcapsules; Manchurian walnut oil; Manchurian walnut protein isolate; wall material; encapsulation efficiency

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