食品科学 ›› 2009, Vol. 30 ›› Issue (2 ): 146-148.doi: 10.7506/spkx1002-6630-200902030

• 工艺技术 • 上一篇    下一篇

三级逆流法提取甜菊糖甙的工艺研究

郁 军1,岳鹏翔1,郁 红2,孙冀平1,郑远斌1   

  1. 1.大闽国际集团研发中心 2. 江苏德发树脂有限公司
  • 收稿日期:2008-12-31 出版日期:2009-01-15 发布日期:2010-12-29
  • 通讯作者: 郁军 E-mail:drjunyu@gmail.com
  • 基金资助:

    福建省科技厅青年人才资助项目(2007F3124);福建省科技厅星火计划重点项目(2008S0020);
    中国博士后科学基金资助项目(20070420966)

Study on Three- stage Continuous Countercurrent Extraction Technology of Steviol Glycosides

YU Jun1,YUE Peng-xiang1,YU Hong2,SUN Ji-ping1,ZHENG Yuan-bin1   

  1. (1. Research and Development Center, Damin International Group, Zhangzhou 363000, China;
    2. Jiangsu Defa Resin Co. Ltd., Yancheng 224300, China)
  • Received:2008-12-31 Online:2009-01-15 Published:2010-12-29
  • Contact: YU Jun1 E-mail:drjunyu@gmail.com

摘要:

本实验首先比较研究了晒干、阴干、烘干、微波干燥等几种不同的干燥方式对甜菊叶中甜菊糖甙的影响。结果表明,微波高火干燥的效果最好,只需3min,甜叶菊鲜叶中的水分从76.07% 降到了3.53% 且叶片颜色保持原色,莱鲍迪甙-A(Rebaudioside A,Reb-A)的含量提高了27%,甜菊苷(Stevioside,Ste)的含量提高了22%;然后比较研究了三级逆流连续提取、三罐串联逆流提取及单罐提取甜菊糖甙的提取效率,结果表明这三种方法的提取得率相近(分别为99.9%、99.82% 及99.9%),但三级逆流连续提取的整个过程只需要20min,而其他两种提取方式整个过程至少需要60min,因此,三级逆流连续提取是一种更加适合于工业化大生产的提取方式。

关键词: 甜叶菊, 甜菊糖甙, 逆流提取, 干燥

Abstract:

This study aimed to develop a continuous operation mode for extracting steviol glycosides from stevia leaves instead of current batch mode by means of three-stage continuous countercurrent extraction technology. Different drying methods of stevia leaves were compared, like insolation, drying in the shade, drying in the oven and microwave drying. The results showed that microwave drying (a rapid drying method) is the best way, which only takes three minutes to dry stevia leaves from the moisture 76.07% to 3.53%, meanwhile, the contents of rebaudioside A and stevioside in the dried leaves are respectively increased by 27% and 22%, respectively. The followed work was comparison of extraction efficiency between the three-stage continuous countercurrent extraction mode and three-stage tandem countercurrent extraction and batch extraction modes. The results demonstrated that the extraction yields of the three methods are closely tied (99.9%, 99.82% and 99.9%), but the whole procedure only takes 20 minutes for the continuous countercurrent extraction, while the other two batch extraction modes take at least 60 minutes respectively. Therefore, the continuous countercurrent extraction is a better and more suitable extraction method for industrial production.

Key words: stevia, steviol glycosides, countercurrent extraction, drying

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