食品科学 ›› 2019, Vol. 40 ›› Issue (4): 21-27.doi: 10.7506/spkx1002-6630-20170831-368

• 食品化学 • 上一篇    下一篇

中链甘油三酯/玉米醇溶蛋白核壳结构微胶囊载体的构建及表征

黄?雪1,王?颖1,张?慧1,赵?萌1,2,*,方亚鹏1,2   

  1. (1.湖北工业大学 菲利普斯亲水胶体研究中心,湖北省食品胶体国际科技合作基地,湖北?武汉 430068;2.工业发酵湖北省协同创新中心,湖北?武汉 430068)
  • 出版日期:2019-02-25 发布日期:2019-03-05
  • 基金资助:
    国家自然科学基金青年科学基金项目(31601514);国家自然科学基金面上项目(31322043); 湖北省科技厅国际合作项目(DWHZ2017000010)

Construction and Characterization of Medium-Chain Triglyceride (MCT)/Zein Microcapsules with Core-Shell Structure

HUANG Xue1, WANG Ying1, ZHANG Hui1, ZHAO Meng1,2,*, FANG Yapeng1,2   

  1. (1. Glyn O. Phillips Hydrocolloid Research Centre, Hubei International Scientific and Technological Cooperation Base of Food Hydrocolloids, Hubei University of Technology, Wuhan 430068, China; 2. Hubei Collaborative Innovation Centre for Industrial Fermentation, Wuhan 430068, China)
  • Online:2019-02-25 Published:2019-03-05

摘要: 以中链甘油三酯(medium-chain triglyceride,MCT)为油相内核,以玉米醇溶蛋白(Zein)为外壳主要成分,低剪切条件下反溶剂法制备大粒径核壳结构的MCT/Zein微胶囊微米载体。通过考察微胶囊载体的宏观形态、微观形态及粒径分布,优化得到微胶囊载体的最佳制备工艺为质量分数0.5%的阿拉伯胶(gum arabic,GA)作为乳化剂、乳化速率800?r/min、Zein沉淀溶液为“30?mL水+100?mL?GA溶液”、Zein沉淀溶液加入速率6?mL/min,并采用扫描电子显微镜、激光共聚焦显微镜、激光粒度分析仪表征冻干MCT/Zein微胶囊载体的结构特征和粒径特性,结果表明该法制备的微胶囊载体具有典型的核壳结构,粒径均一、稳定性良好。本实验建立MCT/Zein核壳结构微胶囊的反溶剂制备法,该法简单易行,适用于多种油溶性活性组分的包埋和保护研究。

关键词: 微胶囊载体, 核壳结构, 反溶剂法, 中链甘油三酯, 玉米醇溶蛋白

Abstract: In this research, medium-chain triglyceride (MCT) and zein were used respectively as internal oil phase (core) and external shell to prepare MCT/zein microcapsules with core-shell structure by the anti-solvent method. Based on the macro-morphology, micro-morphology and size distribution of microcapsules, the optimum preparation conditions were determined as follows: 0.5% gum arabic (GA) as emulsifier, emulsification speed 800 r/min, zein precipitation with a mixture of 30 mL of water and 100 mL of GA solution added at a rate of 6 mL/min. Scanning electron microscopy, confocal laser scanning microscopy and laser particle size analyzer were used to characterize the structure and size properties of freeze-dried MCT/zein microcapsules. It turned out that the MCT/zein microcapsules had a typical core-shell structure with homogenous size distribution and good storage stability. In conclusion, the anti-solvent method was simple, practical and suitable for the preparation of MCT/zein microcapsules with core-shell structure for application in the encapsulation and protection of various lipophilic bioactive components.

Key words: microcapsule carrier, core-shell structure, anti-solvent method, medium chain triglyceride (MCT), zein

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