食品科学 ›› 2024, Vol. 45 ›› Issue (1): 181-190.doi: 10.7506/spkx1002-6630-20230308-079

• 食品工程 • 上一篇    

共封装硒肽和VE微胶囊制备及其理化特性

蔡杰,方媛,贾继来,张碟,丛欣,程水源   

  1. (1.武汉轻工大学硒科学与工程现代产业学院,国家富硒农产品加工技术研发专业中心,湖北省绿色富硒农产品精深加工技术研发工程中心,湖北 武汉 430023;2.武汉轻工大学 大宗粮油精深加工教育部重点实验室,农产品加工与转化湖北省重点实验室,湖北 武汉 430023;3.恩施德源硒材料工程科技有限公司,湖北 恩施 445000)
  • 发布日期:2024-02-05
  • 基金资助:
    湖北省国际科技合作项目(2021EHB029); 武汉轻工大学硒科学与工程现代产业学院-恩施德源硒材料工程科技有限公司技术储备项目(Se1-202111); 赣州市综合检验检测院开放基金课题(GZSZJYKF-202204)

Preparation and Physicochemical Properties of Microcapsules Loaded with Selenium-Enriched Peptides and VE

CAI Jie, FANG Yuan, JIA Jilai, ZHANG Die, CONG Xin, CHENG Shuiyuan   

  1. (1. National R&D Center for Se-rich Agricultural Products Processing, Hubei Engineering Research Center for Deep Processing of Green Se-rich Agricultural Products, School of Modern Industry for Selenium Science and Engineering, Wuhan Polytechnic University, Wuhan 430023, China; 2. Key Laboratory for Deep Processing of Major Grain and Oil, Ministry of Education, Hubei Key Laboratory for Processing and Transformation of Agricultural Products, Wuhan Polytechnic University, Wuhan 430023, China; 3. Enshi Se-Run Material Engineering Technology Co. Ltd., Enshi 445000, China)
  • Published:2024-02-05

摘要: 通过乳化-冷冻干燥联合技术构建微胶囊体系,以实现对具有不同极性的物质(亲水性硒肽和亲脂性VE)的稳态化共封装。以包埋率作为参考,通过单因素试验考察壁材浓度、硒肽和VE含量等工艺参数对包埋效果的影响。傅里叶变换红外光谱和扫描电子显微镜图像表明微胶囊能够有效封装硒肽和VE,并且具有较好的水分散性,复溶后仍保持双重乳液结构。热稳定性分析和2,2’-联氮双(3-乙基苯并噻唑啉-6-磺酸)阳离子自由基清除实验结果证实,相比于硒肽粉末,微胶囊具有更高的热稳定性和抗氧化活性。电子鼻分析结果进一步证实微胶囊体系对硒肽自身异味具有较好的遮掩效果。体外模拟消化实验表明,微胶囊封装提高了硒肽在模拟胃液中的稳定性,并且硒肽在模拟肠液具有更低的保留率,能够被有效释放。相关研究结论将为富硒功能性食品营养补充剂的开发提供理论依据。

关键词: 硒肽;VE;共封装;乳液;微胶囊

Abstract: A microcapsule system for the co-encapsulation of selenium-enriched peptides, being hydrophilic, and vitamin E (VE), being lipophilic, was developed using a combination of emulsification and freeze-drying. The effects of wall material concentration, selenium-enriched peptide content, and VE content on the encapsulation efficiency was investigated by single-factor experiments. Fourier transform infrared (FTIR) spectroscopy and scanning electron microscopy (SEM) showed that the selenium-enriched peptides and VE were effectively encapsulated in the microcapsules, and the microcapsules possessed good water dispersibility and maintained its double emulsion structure after reconstitution. The results of thermal stability analysis and 2,2’-azinobis-(3-ethylbenzthiazoline-6-sulfonic acid) (ABTS) cation radical scavenging assay confirmed that compared with selenium-enriched peptides, the microcapsules had higher thermal stability and antioxidant activity. Furthermore, electronic nose analysis showed that the microcapsule system possessed a good masking effect on the odor of selenium-enriched peptides. In vitro simulated digestion experiments showed that microencapsulation enhanced the stability of selenium-enriched peptides in simulated gastric juice and lowered the retention rate in simulated intestinal fluid; selenium-enriched peptides were effectively released from the microcapsules. This study will provide a theoretical basis for the development of selenium-enriched functional foods and nutritional supplements.

Key words: selenium-enriched peptides; vitamin E; co-encapsulation; emulsion; microencapsulation

中图分类号: