食品科学 ›› 2025, Vol. 46 ›› Issue (24): 226-236.doi: 10.7506/spkx1002-6630-20250617-126

• 成分分析 • 上一篇    

仪器分析结合多元统计法解析复热方式对姜母鸭风味的影响规律

王天泽,成晓瑜,王乐,张凯华,刘博文,赵冰,常思远   

  1. (1.中国肉类食品综合研究中心,北京食品科学研究院,肉类加工技术北京市重点实验室,北京 100068;2.内蒙古塞飞亚农业科技发展股份有限公司,内蒙古 赤峰 024207)
  • 发布日期:2025-12-26
  • 基金资助:
    内蒙古自治区科技计划项目(2023KJHZ0009)

Deciphering the Influence of Reheating Methods on Flavor of Ginger Duck through Instrumental Analysis Coupled with Multivariate Statistics

WANG Tianze, CHENG Xiaoyu, WANG Le, ZHANG Kaihua, LIU Bowen, ZHAO Bing, CHANG Siyuan   

  1. (1. Beijing Key Laboratory of Meat Processing Technology, Beijing Academy of Food Sciences, China Meat Research Center, Beijing 100068, China; 2. Inner Mongolia Saifeiya Agricultural Science and Technology Development Co. Ltd., Chifeng 024207, China)
  • Published:2025-12-26

摘要: 本研究以我国传统菜肴姜母鸭为研究对象,采用固相微萃取-气相色谱-质谱联用、高效液相色谱、电子鼻和电子舌结合多元统计分析解析水浴、炒制和微波3 种复热方式下鸭肉风味变化规律。结果表明,复热后鸭肉香气物质种类增加,但总量减少,其中炒制和微波复热形成的香气物质种类最多(77 种),但水浴复热香气逸散量低、总量最高。电子鼻主成分分析显示水浴复热和复热前鸭肉的香气特征相似,与炒制和微波复热差异显著。偏最小二乘判别分析结合气味活性值筛选出11 种香气物质为关键差异性标志物。滋味分析显示,复热后游离氨基酸含量下降,苦味核苷酸含量上升,鲜、甜味核苷酸含量无显著变化。其中谷氨酸、5’-鸟苷酸、5’-肌苷酸和5’-腺苷酸对鸭肉滋味贡献较大,但偏最小二乘判别分析显示其在各复热方式中无显著差异,导致鸭肉滋味特征相似。本研究结果可为姜母鸭工业化生产的品质控制和复热方式选择提供科学依据。

关键词: 复热;姜母鸭;风味;偏最小二乘判别分析;主成分分析

Abstract: The study investigated the effects of three reheating methods (water bath, stir-frying, and microwave) on the flavor of ginger duck, a traditional Chinese dish, using solid-phase microextraction (SPME) combined with gas chromatography-mass spectrometry (GC-MS), high performance liquid chromatography (HPLC), electronic nose (E-nose), electronic tongue (E-tongue), and multivariate statistical analysis. The results showed that while the number of aroma compounds increased after reheating, their total content decreased. Stir-frying and microwave reheating produced the highest number of aroma compounds (77), whereas water bath reheating resulted in the lowest aroma loss and the highest content of volatile compounds. Principal component analysis of the E-nose data revealed that the aroma characteristics of water bath-reheated samples closely resembled those of fresh samples and were significantly different from those of stir-fried and microwaved samples. Partial least squares-discriminant analysis (PLS-DA) combined with odor activity values (OAVs) identified 11 key aroma compounds as differential markers. Taste analysis indicated a decrease in free amino acid contents and an increase in bitter nucleotide contents after reheating, while umami and sweet nucleotide contents remained largely unchanged. Glutamic acid, 5’-guanylic acid, 5’-inosinic acid, and 5’-adenylic acid contributed significantly to the taste, but PLS-DA showed no significant differences in their levels among reheating methods, resulting in similar taste profiles. These findings provide a scientific basis for quality control and reheating method selection in the industrial production of ginger duck.

Key words: reheating; ginger duck; flavor; partial least squares discriminant analysis; principal component analysis

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