食品科学 ›› 2010, Vol. 31 ›› Issue (6): 172-176.doi: 10.7506/spkx1002-6630-201006039

• 分析检测 • 上一篇    下一篇

电子鼻检测不同贮藏温度下猪肉新鲜度变化

顾赛麒1,王锡昌1,刘 源1 ,*,赵 勇1,张晶晶1,谢 晶1,郑景洲2   

  1. 1.上海海洋大学食品学院 2.法国阿尔法莫斯公司上海代表处
  • 收稿日期:2009-04-27 出版日期:2010-03-15 发布日期:2010-12-29
  • 通讯作者: 刘 源 E-mail:yliu@shou.edu.cn
  • 基金资助:

    国家“863”计划项目(2008AA100804);上海市科委重大科技攻关项目(07dz19508);
    上海市科委启明星计划项目(07QA14047)

Electronic Nose for Measurement of Freshness Change of Chilled Pork during Storage at Different Temperatures

GU Sai-qi1,WANG Xi-chang1,LIU Yuan1,*,ZHAO Yong1,ZHANG Jing-jing1,XIE Jing1,ZHENG Jing-zhou2   

  1. (1. College of Food Science and Technology, Shanghai Ocean University, Shanghai 201306, China;
    2. Alpha M. O. S. Shanghai Representative Office, Shanghai 200336, China)
  • Received:2009-04-27 Online:2010-03-15 Published:2010-12-29
  • Contact: LIU Yuan1 E-mail:yliu@shou.edu.cn

摘要:

采用电子鼻研究冷却猪肉在不同贮藏温度(- 18、0、4、10、20℃)条件下新鲜度变化规律。选用优化后的进样体积(1500μL)进样,对实验数据进行主成分分析(PCA)、货架期模拟及拟合感官评分的偏最小二乘回归分析(PLS)。结果表明:5 种温度条件下贮藏不同时间肉样挥发性气味差异显著,贮藏温度越高肉样新鲜度发生显著下降时刻越早,预测时间分别为336、180、72、48、18h。对4、20℃条件下电子鼻检测数据与感官评分拟合后进行PLS 分析,相关系数分别高达0.9982和0.9998,表明电子鼻能代替感官评定。逐一选取每一根传感器进行PLS 拟合后发现,TA/2、T40/1、T40/2、P30/2、P40/1、P10/2、P10/1 是对不同新鲜度肉样挥发性气味具有良好特异性响应的传感器。

关键词: 电子鼻, 冷却猪肉, 挥发性气味, 新鲜度, 货架期

Abstract:

Electronic nose was used to measure the freshness change of chilled pork during storage at -18, 0, 4, 10 or 20 ℃. Injection volume of minced samples was optimized to be 1500 μL. Principal component analysis (PCA) of volatile odor of chilled pork was conducted. Electronic nose output signal was plotted as a function of storage time to estimate shelf-life of chilled pork stored at different temperatures. Partial least squares regression (PLS-regression) was employed to analyze correlation between electronic nose output signal and sensory evaluation score of volatile odor of chilled pork stored at 4 or 20 ℃. Results showed that there was a significant difference in volatile odor of chilled pork stored for different time at -18, 0, 4, 10 or 20 ℃. Higher storage temperature resulted in earlier occurrence of significant decrease of freshness. The shelf-life of chilled pork stored at the above temperatures was 336, 180, 72, 48 h and 18 h, respectively. The correlation coefficients between electronic nose output signal and sensory evaluation score of volatile odor of chilled pork stored at 4 and 20 ℃ were as high as 0.9982 and 0.9998, respectively, demonstrating that electronic nose is a reliable alternative to sensory evaluation for analysis of volatile odor of chilled pork. Electronic nose sensors TA/2, T40/1, T40/2, P30/2, P40/1, P10/2 and P10/1 were all found to give excellent specific responses to various characteristic odors of pork.

Key words: electronic nose, chilled pork, volatile odor, freshness, shelf-life

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