Simultaneous Determination of Nine Kinds of Phthalates Multiresidues in Food Packaging Materials by HPLC-ESI-MS/MS

doi:10.7506/spkx1002-6630-200912062

FOOD SCIENCE ›› 2009, Vol. 30 ›› Issue (12 ): 270-275.doi: 10.7506/spkx1002-6630-200912062

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Simultaneous Determination of Nine Kinds of Phthalates Multiresidues in Food Packaging Materials by HPLC-ESI-MS/MS

XU Li-guang1，LI Zhuo-kun1，DING Tao2，XU Chuan-lai1,*，SHEN Chong-yu2，MA Wei1，WANG Li-bing1

(1. School of Food Science and Technology, Jiangnan University, Wuxi 214122, China；
2. Jiangsu Entry-Exit Inspection and Quarantine Bureau, Nanjing 210001, China)

Received:2009-04-15 Online:2009-06-15 Published:2010-12-29
Contact: XU Chuan-lai1,*， E-mail:xcl@jiangnan.edu.cn

Abstract

Abstract:

A HPLC-ESI-MS/MS method was developed for the qualitative and quantitative of nine kinids of phthalates multiresidues in food packaging materials HPLC-ESI-MS/MS. Samples were extracted using acetonitrile. The analytes were separated using 0.1% fomic acid-methanol system as the mobile phase with a linear gradient elution program , and determined by a tandem mass detector. The mean recovery for each analyted ranged from 65.28% to 98.33%, with the relative standard deviations from 5.35% to 11.22%, and the limits of detection were about 5－20 ng/ml.

Key words: phthalates, food packaging materials, HPLC-ESI-MS/MS, multi-residues

CLC Number:

TS207.5

XU Li-guang1，LI Zhuo-kun1，DING Tao2，XU Chuan-lai1,*，SHEN Chong-yu2，MA Wei1，WANG Li-bing1XU Li-guang1，LI Zhuo-kun1，DING Tao2，XU Chuan-lai1,*，SHEN Chong-yu2，MA Wei1，WANG Li-bing1. Simultaneous Determination of Nine Kinds of Phthalates Multiresidues in Food Packaging Materials by HPLC-ESI-MS/MS[J]. FOOD SCIENCE, 2009, 30(12 ): 270-275.

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Simultaneous Determination of Nine Kinds of Phthalates Multiresidues in Food Packaging Materials by HPLC-ESI-MS/MS

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