Use of Solid Phase Extraction - Flow Injection- Chemiluminescence for Determination of Sarafloxacin in Eggs

doi:10.7506/spkx1002-6630-201022081

FOOD SCIENCE ›› 2010, Vol. 31 ›› Issue (22): 372-374.doi: 10.7506/spkx1002-6630-201022081

• Analysis & Detection • Previous Articles Next Articles

Use of Solid Phase Extraction - Flow Injection- Chemiluminescence for Determination of Sarafloxacin in Eggs

HUANG Jin-hui，GAO Xiang-yang*

College of Food Science and Technology, Henan Agricultural University, Zhengzhou 450002, China

Received:2010-02-03 Online:2010-11-25 Published:2010-12-29
Contact: GAO Xiang-yang* E-mail:ndgaoxy@163.com

Abstract

Abstract:

A high sensitive and fast method was developed for determination of sarafloxacin(SAR) in eggs. Sarafloxacin in sample was extracted with phosphate, and purified by solid phase extraction (SPE). Since sarafloxacin could significantly enhanced the reaction between luminol and potassium ferricyanide, it could be detected by flow injection-chemiluminescence method. The linear ranges of this method was 6×10-9－6×10-5 mol/L, and the detection limit was 3.97×10-11 mol/L. The average recovery was 96.2%, and the relative stand deviation (RSD) was 1.71%(n=11).

Key words: solid phase extraction, flow injection-chemiluminescence, sarafloxacin, eggs

CLC Number:

O657.3
R917

HUANG Jin-hui，GAO Xiang-yang*. Use of Solid Phase Extraction - Flow Injection- Chemiluminescence for Determination of Sarafloxacin in Eggs[J]. FOOD SCIENCE, 2010, 31(22): 372-374.

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Use of Solid Phase Extraction - Flow Injection- Chemiluminescence for Determination of Sarafloxacin in Eggs

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