Determination of Chloramphenicol Residues in Chichen by SPE-HPLC

Abstract

Abstract: The chloramphenicol in chichen was assayed with the method of solid phase extraction and high performance liquid chromatography (HPLC). The chichen sample was extracted by ethylacetate and cleaned by ENVI-18 SPE column. Then the sample was separated by the C18 column with a mobile phase of methanol and water(35:65, V/V), at the rate of 1ml/min and detected at 278nm. The RSD of this method is less than 5%, and the detection limit was 0.005μg/g.The everage recoveries was 82.4%.

Key words: chloramphenicol residues, chichen, solid phase extraction, high performance liquid chromatography(HPLC)

HE Fang-Yi, LI Tie-Chun, LI Xue-Cheng, XU Ke, HUI Rui-Hua. Determination of Chloramphenicol Residues in Chichen by SPE-HPLC[J]. FOOD SCIENCE, 2006, 27(12): 629-630.

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Determination of Chloramphenicol Residues in Chichen by SPE-HPLC

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