Simultaneous Distillation Extraction and GC-MS Analysis of Volatile Components from China-Hemp Leaves

doi:10.7506/spkx1002-6630-201120047

FOOD SCIENCE ›› 2011, Vol. 32 ›› Issue (20): 226-229.doi: 10.7506/spkx1002-6630-201120047

• Analysis & Detection • Previous Articles Next Articles

Simultaneous Distillation Extraction and GC-MS Analysis of Volatile Components from China-Hemp Leaves

JIANG Yong1，LI Jing-yu1,2，DU Jun-qiang1,3,4，HE Jin-feng3，HE Cong-fen1，ZHU Jun1,*

(1. Beijing Key Laboratory of Plant Resources and Development, School of Food and Chemical Engineering, Beijing Technology and Business University, Beijing 100048, China；2. College of Life Sciences, Capital Normal University, Beijing 00048, China； 3. Research Center of China-Hemp Materials, Quartermaster Research Institute, General Logistic Department of Chinese People, s Liberation Army, Beijing 100082, China；4. College of Food Science and Technology, Sichuan Agricultural University, Ya’an 625014, China)

Online:2011-10-25 Published:2011-10-12

Abstract

Abstract: The volatile components of China-Hemp leaves were analyzed by simultaneous distillation extraction (SDE) coupled to gas chromatography-mass spectrometry (GC-MS). The effect of extraction time on extraction efficiency using dichloromethane as the extraction solvent was examined. The results indicated an operating time of 4 h proved optimal for SDE. A total of 44 compounds were identified from China-Hemp leaves, accounting for 86.04%, including 7 ketones (4.67%), 2 hydroxybenzenes (6.13%), 4 aldehydes (3.88%), 8 alcohols (15.35%), 13 hydrocarbons (29.40%) and 8 other compounds (25.64%). The prevailing compounds were caryophyllene oxide (14.36%), caryophyllene (8.08%) and α-caryophyllene(7.05%).

Key words: China-hemp, simultaneous distillation and extraction (SDE), gas chromatography-mass spectrometry (GC-MS), volatile components

CLC Number:

TS207.3

JIANGYong，LIJing-yu，DUJun-qiang,，HEJin-feng，HECong-fen，ZHUJun. Simultaneous Distillation Extraction and GC-MS Analysis of Volatile Components from China-Hemp Leaves[J]. FOOD SCIENCE, 2011, 32(20): 226-229.

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Simultaneous Distillation Extraction and GC-MS Analysis of Volatile Components from China-Hemp Leaves

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