Key aroma compounds of Yanghe supple and mellow aroma style liquors

Abstract

Abstract:

The total of 66 aroma compounds were determined by headspace solid-phase microextraction followed by GC-MS on the basis of micro volatile compounds and aroma compounds of Yanghe supple and mellow aroma type liquors. Ethyl hexanoate is the key aroma of supple and mellow aroma style liquors by calculation of odor activity values (OAVs) of aroma compounds; OAV is more than 27000, and average OAV of 4 samples is 24799. Ethyl 2-methylbutanoate, dimethyl trisulfide, ethyl pentanoate, ethyl butanoate, and ethyl octanoate are important aroma compounds. Pentanoic acid, ethyl 2-methylpropanoate, 3-methylbutanal, ethyl 3-methylbutanoate, and hexanoic acid contribute to aroma and flavor of Yanghe liquors. The results showed the key aroma compound of supple and mellow aroma type liquor was same to strong aroma type liquor, whereas the important aromas were different.

CLC Number:

TS262.3

References

[1]沈怡方.试论浓香型白酒的流派[J].酿酒,1992,19(5):10-13
[2]范文来; 徐岩.从微量成分分析浓香型大曲酒的流派[J].酿酒科技,2000,101(5):92-94
[3]赵国敢; 陈诚.洋河绵柔型白酒风格浅析[J].酿酒,2009,36(5):21-23
[4]朱广生; 陈翔; 陈亦清; 滕抗.绵柔型白酒研究初探[J].酿酒,2007,34(6):6-10
[5]朱广生; 陈亦清; 陈翔.绵柔型白酒的创新与实践[J].酿酒,2008,35(6):16-18
[6]陈翔; 王亚庆.“洋河蓝色经典”工艺特征、环境因素及微量成分与人体健康的关系[J].酿酒科技,2007,158(8):161-164
[7]Fan W.; Qian, M. C..Headspace solid phase microextraction (HS-SPME) and gas chromatography-olfactometry dilution analysis of young and aged Chinese "Yanghe Daqu" liquors[J].Journal of Agricultural and Food Chemistry,2005,53(20):7931-7938
[8]Fan, W.; Qian, M. C..Identification of aroma compounds in Chinese 'Yanghe Daqu' liquor by normal phase chromatography fractionation followed by gas chromatography/olfactometry[J].Flavour and Fragrance Journal,2006,21(2):333-342
[9]范文来; 徐岩; 杨廷栋; 张雨柏; 朱广生; 周新虎; 陈翔.应用液液萃取与分馏技术定性绵柔型蓝色经典微量挥发性成分[J].酿酒,2012,接收:-
[10]聂庆庆; 徐岩; 范文来.洋河系列绵柔型白酒香气成分研究[J].食品工业科技,2012,接收:-
[11]Gijs L.; Chevance, F.; Jerkovic, V.; Collin, S..How low pH can intensify β-damascenone and dimethyl trisulfide production through beer aging[J].Journal of Agricultural and Food Chemistry,2002,50(20):5612-5616
[12]Gijs L.; Perpète, P.; Timmermans, A.; Collin, S..3-Methylthiopropionaldehyde as precursor of dimethyl trisulfide in aged beers[J].Journal of Agricultural and Food Chemistry,2000,48(12):6196-6199
[13]Fang Y.; Qian, M. C..Sensitive quantification of sulfur compounds in wine by headspace solid-phase microextraction technique[J].Journal of Chromatography A,2005,1080(2):177-185
[14]赵书圣; 范文来; 徐岩; 张国强; 徐钦祥; 李志强.酱香型白酒生产酒醅中呋喃类物质研究[J].中国酿造,2008,21:10-13
[15] Grosch, W..Detection of potent odorants in foods by aroma extract dilution analysis[J].Trends in Food Science & Technology,1993,4(3):68-73
[16]范文来; 徐岩.白酒79个风味化合物嗅觉阈值测定[J].酿酒,2011,38(4):80-84
[17]Poisson L.; Schieberle, P..Characterization of the key aroma compounds in an American Bourbon whisky by quantitative measurements, aroma recombination, and omission studies[J].Journal of Agricultural and Food Chemistry,2008,56:5820-5826
[18] Boonbumrung, S; Tamura, H.; Mookdasanit, J.; Nakamoto, H.; Ishihara, M.; Yoshizawa, T.; Varanyanond, W..Characteritic aroma components of the volatile oil of yellow Keaw mango fruits determined by limited odor unit method[J].Food Science and Technology Research,2001,7(3):200-206
[19]Culleré L.; Escudero, A.; Cacho, J. F.; Ferreira, V..Gas chromatography-olfactometry and chemical quantitative study of the aroma of six premium quality Spanish aged red wines[J].Journal of Agricultural and Food Chemistry,2004,52(6):1653-1660
[20].http://wwwleffingwell.com/esters.htm
[21]Tan Y.; Siebert, K. J..Quantitative structure-activity relationship modeling of alcohol, ester, aldehyde, and ketone flavor thresholds in beer from molecular features[J].Journal of Agricultural and Food Chemistry,2004,52(10):3057-3064
[22]Peinado R. A.; Mauricio, J. C.; Medina, M.; Moreno, J. J..Effect of Schizosaccharomyces pombe on aromatic compounds in dry sherry wines containing high levels of gluconic acid[J].Journal of Agricultural and Food Chemistry,2004,52:4529-4534
[23] Karahadian, C; Josephson, D. B.; Lindsay, R. C..Volatile compounds from Penicillium sp. contributing musty-earthy notes to Brie and Camembert cheese flavors[J].Journal of Agricultural and Food Chemistry,1985,33:339-343
[24]Guth H..Quantitation and sensory studies of character impact odorants of different white wine varieties[J].Journal of Agricultural and Food Chemistry,1997,45(8):3027-3032