FOOD SCIENCE ›› 2011, Vol. 32 ›› Issue (18): 243-245.doi: 10.7506/spkx1002-6630-201118053

• Analysis & Detection • Previous Articles     Next Articles

Uncertainty Evaluation for Cadmium Determination in Flour by Graphite Furnace Atomic Absorption Spectrometry

FAN Hui-ping1,JI Jian-sheng2,FU Feng2,GAO Jing-ming2,ZHAO Yu-yu1   

  1. (1. College of Food Science and Technology, Henan Agricultural University, Zhengzhou 450002, China; 2. Henan Station for Supervision and Inspection of Grain, Oil and Feed Product Quality, Zhengzhou 450008, China)
  • Received:2018-06-20 Revised:2018-06-20 Online:2011-09-25 Published:2011-09-24

Abstract: The content of cadmium in flour was determined by graphite furnace atomic absorption spectrometry (GFAAS), and the sources of uncertainty were evaluated. Each parameter in mathematic model was analyzed to evaluate the type A and type B uncertainties in the method. To obtain the uncertainty evaluation, each uncertainty component was synthesized and extended by the current international method. The results showed that the major source of the uncertainty in the method was the sample solution volume and the standard curve.

Key words: uncertainty, cadmium, graphite furnace atomic absorption spectrometry

CLC Number: