FOOD SCIENCE ›› 2010, Vol. 31 ›› Issue (20): 367-370.doi: 10.7506/spkx1002-6630-201020076

• Analysis & Detection • Previous Articles     Next Articles

Rapid Determination of Total Organic Matter in Food Plastic Bag by Flow Injection Coupled with Chemiluminescence

WANG Chang-qing,GAO Xiang-yang*,SHI Han-yu   

  1. College of Food Science and Technology, Henan Agricultural University, Zhengzhou 450002, China
  • Received:2010-04-23 Revised:2010-09-07 Online:2010-10-25 Published:2010-12-29
  • Contact: GAO Xiang-yang E-mail:ndgaoxy@163.com

Abstract:

The aim of the present study was to develop a novel analytical method for rapidly determining total organic matter in food plastic bag using flow injection coupled with chemiluminescence. Samples received ultrasonic-assisted extraction and subsequent microwave pressure digestion prior to the analysis with luminol-H2O2-Cr3+ flow injection chemiluminescence system. Chromium (Ⅲ) (considered equivalent to total organic matter) displayed a linear range of 1.154×10-10 to 1.154×10-5 mol/L (1/3Cr3+) and a detection limit of 4.476×10-11 mol/L (1/3Cr3+), with a relative standard deviation (RSD) of 3.1% (n = 3). The proposed method is characterized by high sensitivity, ease of operation, rapid determination and low cost. All these figures of merits benefit its promotion and popularization.

Key words: flow injection analysis, chemiluminescence, luminol system, food plastic bag, total organic matter

CLC Number: