FOOD SCIENCE ›› 2012, Vol. 33 ›› Issue (8): 184-187.doi: 10.7506/spkx1002-6630-201208039

• Analysis & Detection • Previous Articles     Next Articles

Rapid Determination of Bisphenol A in Nursing Bottles by Flow Injection Inhibitory Chemiluminescence Analysis

GAO Xiang-yang,WANG Chang-qing   

  1. (College of Food Science and Technology, Henan Agricultural University, Zhengzhou 450002, China)
  • Online:2012-04-25 Published:2012-03-31

Abstract: In order to establish a new rapid method for determining bisphenol A (BPA) in nursing bottles, cut pieces of nursing bottles were extracted with high-purity water under ultrasonic assistance, and the extracted analyte was enriched by solid phase extraction and determined using a uminol-H2O2-Cr chemiluminescence system. The esults showed that the chemiluminescence system was inhibited by BPA. An excellent linear relationship was observed in the range of 2.0 × 10-9 -1.0 × 10-5 mol/L. The detection limit was 4.6 × 10-10 mol/L. The average spike recoveries of BPA in 5 types of commercial samples were in the range of 95.4%-106.8%, and the relative standard deviations for 7 parallel determinations were all less than 4%. The method had the advantages of sensitivity, simplicity, rapidity, low cost and accuracy over the Chinese national standard method, thus being worth promoting and popularizing.

Key words: flow injection analysis (FIA), chemiluminescence, luminol, nursing bottle, bisphenol A

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