食品科学 ›› 2010, Vol. 31 ›› Issue (22): 442-444.doi: 10.7506/spkx1002-6630-201022099

• 分析检测 • 上一篇    下一篇

芹菜叶挥发油化学成分的GC/MS分析

孙小媛,李铁纯,周 雪   

  1. 鞍山师范学院化学系
  • 收稿日期:2010-07-01 修回日期:2010-10-22 出版日期:2010-11-25 发布日期:2010-12-29
  • 通讯作者: 孙小媛 E-mail:sunxiaoyuan12@126.com

GC-MS Analysis of Volatile Components in Celery Leaves

SUN Xiao-yuan,LI Tie-chun,ZHOU Xue   

  1. Department of Chemistry, Anshan Normal University, Anshan 114007, China
  • Received:2010-07-01 Revised:2010-10-22 Online:2010-11-25 Published:2010-12-29
  • Contact: SUN Xiao-yuan E-mail:sunxiaoyuan12@126.com

摘要:

为比较不同地区芹菜叶挥发油的化学组成,采用水蒸气蒸馏方法对产自辽宁3 个不同地区芹菜叶的挥发性成分进行提取,并采用GC-MS 方法对提取的挥发性成分进行鉴定。结果从3 种芹菜叶中一共鉴定出32 种挥发性化学成分,其中鞍山芹菜叶中鉴定出12 种,其含量占挥发油的27.29%,特有成分为β-月桂烯、n-十六酸、9,12,15-十八碳三烯酸等;抚顺芹菜叶中鉴定出16 种,其含量占挥发油的21.78%,特有成分为苯酚、桉叶双烯、5-(1,5-二甲基-4- 己基)-2- 甲基-1,3- 环己二烯等;北票芹菜叶中鉴定出9 种,其含量占挥发油的12.59%,特有成分为桉叶双烯、邻苯二甲酸二丁酯、十八烷等。

关键词: 芹菜叶, 挥发性成分, 气相色谱- 质谱法(GC-MS)

Abstract:

In order to compare chemical compositions of essential oil in celery leaves from different areas, essential oil in celery leaves from 3 areas in Liaoning province was extracted by using steam distillation method and the compositions of essential oil were identified by gas chromatography-mass spectroscopy (GC-MS). Totally 32 kinds of volatile compounds were identified in celery leaves from 3 areas. A total of 12 kinds of volatile compounds including characteristic compounds of β-myrcene, nhexadecanoic acid and 9, 12, 15-octadecadienoic acid were identified in celery leaves from Anshan, which was accounted for 27.29% of total volatile oil. Sixteen kinds of volatile compounds such as phenol and 5-(1,5-dimethyl-4-hexyl)-2-methyl-1,3-cyclohexadiene as the characteristic components were identified in celery leaves from Fushun, which was accounted for 21.78% of total volatile oil. Nine volatile compounds including special compounds of diene, dibutyl phthalate and octadecane were identified in Baiqiao celery leaves with 12.59% of total volatile oil.

Key words: celery leaves, volatile oil, gas chromatography-mass spectrometry (GC-MS)

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