食品科学 ›› 2009, Vol. 30 ›› Issue (12): 251-253.doi: 10.7506/spkx1002-6630-200912057

• 分析检测 • 上一篇    下一篇

乌榄果实挥发性化学成分的GC-MS分析

郭守军1,杨永利1,黄佳红1,谢秋玲2,佘建保1,黄妙凤1   

  1. 1.韩山师范学院生物系 2.暨南大学生物工程研究所
  • 收稿日期:2008-09-08 修回日期:2008-11-30 出版日期:2009-06-15 发布日期:2010-12-29
  • 通讯作者: 郭守军 E-mail:sjguo2006@yahoo.com.cn
  • 基金资助:

    广东省科技攻关项目(2007B080701046);国家星火计划项目(2006EA780088)

GC-MS Analysis of Chemical Constituents of Volatile Oil from Fruits of Canarium pimela Leenh.

GUO Shou-jun1,YANG Yong-li1,HUANG Jia-hong1,XIE Qiu-ling2,SHE Jian-bao1,HUANG Miao-feng1   

  1. (1. Department of Biology, Hanshan Normal University, Chaozhou 521041, China;
    2. Institute of Bioengineering, Jinan University, Guangzhou 510632, China)
  • Received:2008-09-08 Revised:2008-11-30 Online:2009-06-15 Published:2010-12-29
  • Contact: GUO Shou-jun1, E-mail:sjguo2006@yahoo.com.cn

摘要:

采用水蒸气蒸馏法对乌榄果实挥发油进行提取,运用毛细管气相色谱- 质谱联用法结合计算机检索对乌榄果实挥发油进行成分分析和鉴定,经毛细管色谱分离出43 个峰,共确认了其中41 种化合物,所鉴定化合物的含量占全油的97.8%。用气相色谱面积归一化法测定了各组分的相对百分含量。其化学成分主要为:1- 甲基-2-(1- 甲乙基) 苯、D- 柠檬烯、α- 侧柏烯、α- 蒎烯、己酸、己醛、石竹烯、氧化石竹烯、1- 戊醇、1- 己醇、β - 水芹烯、古巴烯、α- 蛇麻烯、2- 戊基- 呋喃、壬醛、杜松烯、(-)- 斯帕苏烯醇和[1R-1 α,4a β,8a α]- 十氢-1,4a- 二甲基-7-(1- 甲基乙缩醛基)-1- 萘醇,以上十六种化合物占其挥发油总量的85.88%。

关键词: 乌榄, 挥发油成分, 气相色谱—质谱联用

Abstract:

Essential oil from fruits of Canarium pimela Leenh. was extracted by steam distillation and analyzed by capillary GC-MS method combined with computer retrieval. More than 43 peaks were isolated and 41 compounds were identified, which accounted for 97.8% of the total essential oil. The relative percentages of these compounds identified were determined by GC area normalization method. The main chemical components were 1-methyl-2-(1-methylethyl)-benzene, D-limonene, α- Phellandrene, α-pinene, hexanoic acid, hexanal, caryophyllene, caryophyllene oxide, 1-pentanol, 1-hexanol, β-phellandrene, copaene, α-humulene, 2-pentyl-furan, nonanal, cadinene, (-)-spathulenol and decahydro-1,4a-dimethyl-7-(1-methylethylidene)- [1R-(1α,4aβ,8aα)]-naphthalenol, which accounted for 85.88% of the total essential oil.

Key words: Canarium pimela Leenh., essential oil, GC-MS

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