食品科学 ›› 2010, Vol. 31 ›› Issue (14): 272-274.doi: 10.7506/spkx1002-6630-201014062

• 分析检测 • 上一篇    下一篇

几种常见菜籽中钙的含量及溶出度测定

蔡广知,沈晓君,孙全乐,郭金萍,郭云龙,贡济宇*   

  1. 长春中医药大学药学院
  • 收稿日期:2009-10-21 修回日期:2010-04-02 出版日期:2010-07-15 发布日期:2010-12-29
  • 通讯作者: 贡济宇* E-mail:giy0431@126.com

Calcium Content and Dissolution Rate of Rapeseed

CAI Guang-zhi,SHEN Xiao-jun,SUN Quan-le,GUO Jin-ping,GUO Yun-long,GONG Ji-yu*   

  1. College of Pharmaceutical, Changchun University of Chinese Medicine, Changchun 130117, China
  • Received:2009-10-21 Revised:2010-04-02 Online:2010-07-15 Published:2010-12-29
  • Contact: GONG Ji-yu* E-mail:giy0431@126.com

摘要:

目的:测定几种常见菜籽中钙的含量及溶出度。方法:采用仿生提取- 原子吸收分光光度法(BE-AAS 法)测定菜籽中钙的含量并计算其溶出度。结果:萝卜籽的含钙量较高;黑南瓜籽和葫芦籽粉的溶出度是黄瓜籽粉和苦瓜籽粉的两倍。钙在3~21μg/mL 范围内线性关系良好,相关系数为0.9997,平均回收率为103.58%,RSD 为1.27%。结论:BE-AAS 法可准确测定菜籽中钙的含量及溶出度,菜籽粉可作为钙源。

关键词: BE-AAS法, 菜籽, 钙含量, 溶出度

Abstract:

Bionic extraction followed by atomic absorption spectrometry (BE-AAS) was used to determine the content and dissolution rate of calcium in rapeseed. Turnip seeds contained higher calcium content than the seeds of cucumber, bitter gourd, Perilla, black sesame, black pumpkin, grape, Cucurbitaceae and white gourd. The dissolution rates of black pumpkin and Cucurbitaceae seeds were almost 2 times higher than those of cucumber and bitter gourd seeds. The method exhibited good linearity over the concentration range from 3 to 21μg/mL, with a correlation coefficient of 0.9997. The average recovery for calcium was 103.58%, with a RSD of 1.27%. This method can allow accurate determination of the content of dissolution rate of calcium plant seeds. The seeds of the plants tested are abundant in calcium.

Key words: BE-AAS, plant seeds, calcium content, dissolution

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