食品科学 ›› 2011, Vol. 32 ›› Issue (20): 30-33.doi: 10.7506/spkx1002-6630-201120007

• 工艺技术 • 上一篇    下一篇

八角茴香中精油和莽草酸的提取工艺优化

李 健1,杨 慧1,黎晨晨1,张若男2   

  1. 1.哈尔滨商业大学食品工程学院,黑龙江省高校食品科学与工程重点实验室 2.黑龙江护理高等专科学校
  • 出版日期:2011-10-25 发布日期:2011-10-12

Simultaneous Extraction of Volatile Oil and Shikimic Acid from Star Anise

LI Jian1,YANG Hui1,LI Chen-chen1,ZHANG Ruo-nan2   

  1. (1. Key Laboratory of Food Science and Engineering of Heilongjiang Province, College of Food Engineering, Harbin University of Commerce, Harbin 150076, China;2. Heilongjiang Junior College of Nursing, Harbin 150036, China)
  • Online:2011-10-25 Published:2011-10-12

摘要: 以八角茴香为原料,采用水蒸气蒸馏法提取茴香油和莽草酸。以茴香油和莽草酸得率为指标考察不同粒径、料液比、提取时间、提取温度对茴香油和莽草酸得率的影响。通过单因素和正交试验,确定八角茴香油和莽草酸提取最佳工艺条件为物料粒径80目、料液比1:15(g/mL)、提取温度150℃、提取时间4h。在此最佳工艺条件下,精油得率6.69%,莽草酸得率2.05%。

关键词: 八角茴香, 精油, 莽草酸, 水蒸气蒸馏

Abstract: Steam distillation extraction was used to simultaneously extract the volatile oil and shikimic acid in star anise. In terms of the yields of volatile oil and shikimic acid, the process conditions material granularity, solid-to-liquid ratio, temperature and extraction time were optimized using one-factor-at-a-time combined with orthogonal array design method to be 80 mesh, 1:15 (g/mL), 150 ℃ and 4 h, respectively. Under the optimal conditions, the volatile yield was 6.69% and the shikimic acid 2.05%.

Key words: star anise, volatile oil, shikimic acid, steam distillation extraction

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