食品科学 ›› 2025, Vol. 46 ›› Issue (19): 47-56.doi: 10.7506/spkx1002-6630-20250319-144

• 基础研究 • 上一篇    

玉米醇溶蛋白基甘油包油乳液凝胶的制备与性能表征

李恩泽,马胤果,李佳,鹿瑶,毛立科   

  1. (1.四川成都中农大现代农业产业研究院,四川 成都 611430;2.中国农业大学食品科学与营养工程学院,北京 100083)
  • 发布日期:2025-09-16
  • 基金资助:
    四川省自然科学基金项目(2024NSFSC0369)

Preparation and Characterization of Zein-Based Oil-in-Glycerol Emulsion Gel

LI Enze, MA Yinguo, LI Jia, LU Yao, MAO Like   

  1. (1. CAU-SCCD Advanced Agricultural & Industrial Institute, Chengdu 611430, China; 2. College of Food Science & Nutritional Engineering, China Agricultural University, Beijing 100083, China)
  • Published:2025-09-16

摘要: 以玉米醇溶蛋白为主要原料,通过中等温度诱导法制备甘油包油型无水乳液凝胶,探究其结构组成(玉米醇溶蛋白含量与玉米油含量)对乳液凝胶形成与结构性能的影响。研究发现增加玉米醇溶蛋白质量分数(4%~8%)可以增强连续相网络结构,进而显著提高凝胶强度,使凝胶硬度从(3.43±0.14)N增加至(8.15±0.13)N,凝胶持油力由(97.64±0.21)%上升至100%,持溶剂力由(84.15±0.38)%提高至(96.34±1.20)%。玉米油质量分数的增加(50%~70%)对凝胶强度的改变并不显著,但能够增强乳液凝胶黏度与触变回复性能。同时凝胶中油滴的紧密排列显著提高了乳液凝胶稳定性,使得凝胶的持油力((95.51±0.56)%~(99.17±0.85)%)和持溶剂力((83.29±2.23)%~(93.39±1.01)%)始终保持较高水平。所有配方比例均能形成稳定的乳液凝胶且具有良好的温度响应行为。实验结果证明,通过中等温度法能够有效制备玉米醇溶蛋白基的乳液凝胶,并且可以通过调节蛋白与玉米油的含量实现对凝胶性能的调控,实验结果可为玉米醇溶蛋白乳液凝胶在食品中的实际应用提供理论依据,从而有效提高玉米醇溶蛋白的综合利用度。

关键词: 玉米醇溶蛋白;甘油;乳液凝胶;性能表征;中等温度诱导法

Abstract: In this study, anhydrous zein-based oil-in-glycerol emulsion gels were prepared by a medium temperature induction method. The impact of zein and corn oil contents on the formation and structure of emulsion gels was explored. It was found that increasing the content of zein (4%–8%) enhanced the continuous phase network structure and therefore significantly improved the gel strength, increasing the gel hardness from (3.43 ± 0.14) to (8.15 ± 0.13) N, the oil-holding capacity from (97.64 ± 0.21)% to 100%, and the solvent-holding capacity from (84.15 ± 0.38)% to (96.34 ± 1.20)%. The increase in corn oil content (50%–70%) did not significantly change the gel strength, but enhanced the gel viscosity and thixotropic recovery performance. Meanwhile, the gel stability was improved by the tight arrangement of oil droplets, and the gel oil-holding capacity and solvent-holding capacity were maintained at high levels, (95.51 ± 0.56)%–(99.17 ± 0.85)% and (83.29 ± 2.23)%–(93.39 ± 1.01)%, respectively. All formulations formed stable emulsion gels with good temperature response behavior. Our results proved that the gel properties could be regulated by adjusting the contents of zein and corn oil. This study provides a theoretical basis for the practical application of zein-based emulsion gels in foods, improving the comprehensive utilization rate of zein.

Key words: zein; glycerol; emulsion gel; performance characterization; medium temperature induction method

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