食品科学 ›› 2006, Vol. 27 ›› Issue (11): 283-286.

• 工艺技术 • 上一篇    下一篇

尤曼桉中芦丁的提取方法研究

 曾荣,  罗学刚   

  1.  西南科技大学
  • 出版日期:2006-11-15 发布日期:2011-11-28

Study on Rutin Extraction from Eucalyptus Youmanii

 ZENG  Rong,   Luo-Xue-Gang   

  1. Southwest University of Science and Technology,Mianyang 621000,China
  • Online:2006-11-15 Published:2011-11-28

摘要: 本文首次报道了尤曼桉(EucalyptusYoumanii)芦丁的提取方法和工艺条件。采用正交试验设计分别以碱溶酸沉法、乙醇回流法、热水法提取尤曼桉叶芦丁。碱溶酸沉法的工艺条件为固液比1:10,提取时间10min,pH8,提取两次,热水纯化;乙醇回流法提取尤曼桉芦丁的工艺条件为乙醇浓度75%,提取温度75℃,提取时间3h,碳酸氢纳用量10%,固液比1:20,热水纯化;热水提取尤曼桉芦丁的工艺条件为固液比1:30,时间30min,粒度100目,提取两次,热乙醇纯化。三种提取方法以碱溶酸沉法较优。

关键词:  , 尤曼桉, 芦丁, 提取

Abstract: The method and technique of rutin extraction from Eucalyptus Youmanii leaves were discussed first time in this paper. Rutin was extracted by alkali-solution and acid-isolation,ethyl alcohol reflux and hot water with orthogonal design. The techniques of extracting by alkali-solution and acid-isolation were: pH8,ratio of solid to liquid 1:10,time 10min,extracting twice and purifyed by hot water. The techniques of extracting by ethyl alcohol reflux were: 75% ethyl alcohol,temperature 75℃,time 3h,10% sodium bicarbonate,ratio of solid to liquid 1:20,and purifyed by hot water. The techniques of extracting by hot water were: time 30min,size 100 eyes,ratio of solid to liquid 1:30,extracting twice,and purifyed by hot ethyl alcohol. The method of alkali-solution and acid-isolation extraction is the best among all.

Key words:  , Eucalyptus Youmanii; rutin; extraction;