食品科学 ›› 2008, Vol. 29 ›› Issue (9): 526-528.

• 分析检测 • 上一篇    下一篇

应用微波消解/ICP-OES法测定牦牛肉中的微量元素

 张玉玉, 唐善虎, 胡子文   

  1. 成都理工大学材料与生物工程学院; 西南民族大学生命科学与技术学院;
  • 出版日期:2008-09-15 发布日期:2011-12-08

Determination of Trace Elements in Yak Meat by Microwave Digestion/ICP-OES Method

 ZHANG  Yu-Yu, TANG  Shan-Hu, HU  Zi-Wen   

  1. 1. College of Materials and Bioengineering,Chengdu University of Technology,Chengdu 610059,China; 2. College of Life Science and Technology,Southwest University for Nationalities,Chengdu 610041,China
  • Online:2008-09-15 Published:2011-12-08

摘要: 采用微波消解-电感耦合等离子体发射光谱法(ICP-OES)测定了牦牛肉中的6种微量元素。方法对各元素的检出限为0.0005~0.0120mg/L,相对标准偏差1.50%~4.25%,加标回收实验的回收率为98.55%~102.27%。分析结果表明,牦牛肉中含有人体必须的6种微量元素,含量分别为Cu1.41mg/kg,Zn18.70mg/kg,Ni0.73mg/kg,Mn0.43mg/kg,Mo0.85mg/kg和Co0.29mg/kg。

关键词: 微波消解, 电感耦合等离子发射光谱, 牦牛, 微量元素

Abstract: Microwave digestion- inductively coupled plasma optical emission spectrometer (ICP-OES) method was adopted for the determinations of 6 kinds of trace elements in yak meat. The detection limit of each element is from 0.0005 to 0.0120 mg/L, the relative standard deviation is from 1.50% to 4.25%, and the recovery ratio of spiked sample is from 98.55% to 102.27%. These results showed that the microwave digestion combined with ICP-OES is a sensitive method for the determination of trace elements in meat, and also indicats that yak meat contains Cu 1.41 mg/kg, Zn 18.70 mg/kg, Ni 0.73 mg/kg, Mn 0.43 mg/kg, Mo 0.85 mg/kg, and Co 0.29mg/kg, 6 kinds of essential elements for human.

Key words: microwave digestion, inductively coupled plasma emission spectrometry, yak, trace element