食品科学 ›› 2020, Vol. 41 ›› Issue (8): 194-201.doi: 10.7506/spkx1002-6630-20190528-341

• 成分分析 • 上一篇    下一篇

基于GC-MS、DSA结合PLSR研究羊脂处理方式对热反应体系风味形成的影响

马雪平,詹萍,田洪磊,未志胜,李凯旋   

  1. (1.石河子大学食品学院,新疆 石河子 832000;2.陕西师范大学食品工程与营养科学学院,陕西 西安 710119)
  • 出版日期:2020-04-25 发布日期:2020-04-20
  • 基金资助:
    “十三五”国家重点研发计划重点专项(2016YFD0400705);陕西省重点研发计划一般项目(2019NY-147); 中央高校基金重点项目(GK202002004)

Effects of Mutton Tallow Subjected to Different Treatments on Aroma Compounds Generated from Thermal Reaction Systems as Evaluated by Gas Chromatography-Mass Spectrometry, Descriptive Sensory Analysis and Partial Least Squares Regression

MA Xueping, ZHAN Ping, TIAN Honglei, WEI Zhisheng, LI Kaixuan   

  1. (1. College of Food, Shihezi University, Shihezi 832000, China;2. College of Food Engineering and Nutritional Science, Shaanxi Normal University, Xi’an 710119, China)
  • Online:2020-04-25 Published:2020-04-20

摘要: 采用气相色谱-质谱联用结合描述性感官评价,对以原料羊脂和4 种不同处理方式(酶解、低温氧化、酶解-低温氧化、高温氧化)羊脂为前体制备的模式美拉德反应产物风味特性进行分析鉴定。结果表明,在热反应过程中羊脂处理方式对于热反应产物羊肉特征风味呈现显著差异,其中通过酶解-低温氧化羊脂制备的羊肉风味基料MRP4,表现出明显的肉香味、羊肉味和脂香,同时亦产生种类较多的羊肉特征香气组分,如壬醛、苯甲醛、硫代乙酸乙酯、邻苯二甲酸二丁酯、2-己基噻吩、2-庚基噻吩、2-乙酰基呋喃、2-正戊基呋喃、2,6-二叔丁基-4-甲基苯酚等。结合偏最小二乘回归分析进一步确证酶解-低温氧化处理的羊脂是赋予热加工体系羊肉风味最适风味前体。

关键词: 羊脂, 美拉德体系, 描述性感官分析, 气相色谱-质谱, 偏最小二乘回归分析

Abstract: Gas chromatography-mass spectrometry (GC-MS) and descriptive sensory analysis (DSA) were used to analyze and identify the flavor characteristics of the Maillard reaction products (MRPs) prepared from native and modified mutton tallow (subjected to enzymatic hydrolysis, low temperature oxidation, their combination or high temperature oxidation). The results showed that there was a significant difference in the flavor characteristics of the four MRPs. The MRPs prepared from mutton tallow subjected to enzymatic hydrolysis and mild thermal oxidization showed obvious meaty, muttony and fatty aromas, and contained a variety of characteristic muttony aroma components, including nonanal, benzaldehyde, S-ethyl ethanethioate, dibutyl phthalate, 2-hexylthiophene, 2-heptylthiophene, 2-acetylfuran, 2-n-pentylfuran, and 2,6-di-tert-butyl-4-methylphenol. It was further confirmed by partial least squares regression (PLSR) analysis that mutton tallow subjected to enzymatic hydrolysis and mild thermal oxidization was the most suitable flavor precursor.

Key words: mutton tallow, Maillard reaction system, descriptive sensory analysis, gas chromatography-mass spectrometry, partial least squares regression analysis

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