Macroporous Resin Adsorption for Purification of Crude Oleuropein Extracted from Syringa pubescens Turcz.

doi:10.7506/spkx1002-6300-201008013

FOOD SCIENCE ›› 2010, Vol. 31 ›› Issue (8): 56-59.doi: 10.7506/spkx1002-6300-201008013

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Macroporous Resin Adsorption for Purification of Crude Oleuropein Extracted from Syringa pubescens Turcz.

DENG Rui-xue，LIU Pu，YUAN Hua，ZHAO You-man，DUAN Wen-lu，YIN Wei-ping*

(School of Chemical Engineering and Pharmaceutics, Henan University of Science and Technology, Luoyang 471003, China)

Received:2009-06-16 Revised:2009-10-22 Online:2010-04-15 Published:2010-12-29
Contact: YIN Wei-ping E-mail:ywpq@163.com

Abstract

Abstract:

Macroporous resin adsorption was used to obtain high-purity oleuropein from Syringa pubescens Turcz., an effective antihepatic fibrosis component. Six common macroporous absorption resins were compared for differences in adsorption and desorption performance. D-101 resin was found to be the best choice for oleuropein purification. To achieve an optimal oleuropein purification, the adsorption and desorption characteristics of D-101 resin were investigated. Results showed that the purity of purified crude Syringa pubescens Turcz. oleuropein using D-101 resin under optimized adsorption-desorption conditions was more than 30%. Forty percent aqueous ethanol solution was a fast and effective solvent for oleuropein desorption. D-101 resin exhibited good reusability. This method is easy and convenient in operation and has promising potential for industrial application.

Key words: Syringa pubesceus Turcz, oleuropein, macroporous absorption resin, HPLC

CLC Number:

R284.2

DENG Rui-xue，LIU Pu，YUAN Hua，ZHAO You-man，DUAN Wen-lu，YIN Wei-ping*. Macroporous Resin Adsorption for Purification of Crude Oleuropein Extracted from Syringa pubescens Turcz.[J]. FOOD SCIENCE, 2010, 31(8): 56-59.

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Macroporous Resin Adsorption for Purification of Crude Oleuropein Extracted from Syringa pubescens Turcz.

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