FOOD SCIENCE ›› 2009, Vol. 30 ›› Issue (10): 29-32.doi: 10.7506/spkx1002-6630-200910001

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Preparation and Characterization of β-cyclodextrin Inclusion Compound of Essential Oil from Rosa damascena Miller

WEN Zhen1,LIU Bo1,ZHENG Zong-kun1,YOU Xin-kui1,PU Yi-tao1,LI Qiong2   

  1. (1. College of Chemistry and Chemical Engineering, Shenzhen University, Shenzhen 518060, China;
    2. School of Chemistry and Chemical Engineering, South China University of Technology, Guangzhou 510640, China)
  • Received:2008-07-22 Revised:2008-10-13 Online:2009-05-15 Published:2010-12-29
  • Contact: WEN Zhen1 E-mail:wenzhen1977@163.com

Abstract:

In order to improve the solubility in water and stability of essential oil from Rosa damascena Miller, the essential oil was included with β-cyclodextrin(β-CD) by saturated water solution-stirring method. The inclusion conditions were optimized through orthogonal test, and the inclusion compound was characterized by thin-layer chromatography (TLC), gas chromatography-mass spectrometry (GC-MS), Fourier transform infrared (FTIR) spectrometry and differential scanning calorimetry (DSC). The results showed that the optimal inclusion conditions of essential oil from Rosa damascena Miller were as following: mass ratio of essential oil to β-CD 1:10, inclusion temperature 60 ℃, and inclusion time 2 h. The inclusion ratio of essential oil was up to 80% under above conditions. The inclusion compound retained the main characteristic components of the essential oil and obviously improved its solubility in water and stability. This β-CD inclusion compound of essential oil from Rosa damascena Miller can be used as a solid immediate for the development of functional foods.

Key words: essential oil, Rosa damascena Miller, β-cyclodextrin, inclusion

CLC Number: