Optimization of Synthesis of Soluble Soybean Polysaccharide-Iron (II) Complex by Response Surface Methodology

doi:10.7506/spkx1002-6630-201210020

Abstract

Abstract: In order to optimize the synthesis process of soluble soybean polysaccharide-iron (Ⅱ) complex, based on the single factor tests, a dual quadratic rotary combination design was used to analyze the effects of mass ratio between soluble soybean polysaccharide and catalyst sodium citrate, pH, reaction time and reaction temperature on iron content of SSPS-Fe (Ⅱ). A prediction model was established. The analysis of variance revealed that mass ratio and pH could significantly affect iron content of SSPS-Fe (Ⅱ). The optimal synthesis conditions were mass ratio between soluble soybean polysaccharide and catalyst sodium citrate of 1.89:1, pH 3.89, reaction time of 1.56 h and reaction temperature of 60.6 ℃. The iron content predicted by the model was 23.08%, which was consistent with the experimental value.

Key words: soluble soybean polysaccharide, ferrous, synthesis, response surface methodology

CLC Number:

TQ929.2

HERui-xue，GAOWen-hong，ZENGXin-an，ZHUSi-ming. Optimization of Synthesis of Soluble Soybean Polysaccharide-Iron (II) Complex by Response Surface Methodology[J]. FOOD SCIENCE, 2012, 33(10): 98-102.

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Optimization of Synthesis of Soluble Soybean Polysaccharide-Iron (II) Complex by Response Surface Methodology

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