Simultaneous Determination of Bromate, Chlorite, Chlorate and Common Inorganic Anions in
Drinking Water by Ion Chromatography

doi:10.7506/spkx1002-6630-201212044

Abstract

Abstract: An analytical method for the simultaneous determination of bromate, chlorite, chlorate and common inorganic anions in drinking water was developed using large-volume direct injection and chemically suppressed ion chromatography (IC). An IonPac AS9-HC separation column and an IonPac AG9-HC protection column were used. The mobile phase was 12 mmol/L Na2CO3 at a flow rate of 1.0 mL/min. The injection volume was 100μL. Ten anions could be detected by the method within 18 min with average spike recovery of 93.0%～103.1% (n = 5). The correlation coefficients of calibration curve were 0.9993～0.9999. This method was sensitive, accurate and rapid. It has been applied to determine Kunming tap water and a variety of commercial drinking water with satisfying results.

Key words: ion chromatography, drinking water, bromate, inorganic anions

CLC Number:

O611.5

YANG Min，XIE Jing，YANG Shu-ke，CHEN Hai-yun，WANG Hong-bin. Simultaneous Determination of Bromate, Chlorite, Chlorate and Common Inorganic Anions in Drinking Water by Ion Chromatography[J]. FOOD SCIENCE, 2012, 33(12): 219-222.

[1]	ZHANG Hao, JIANG Xiaohong, HUO Zongli. Determination of Chlorate and Perchlorate in Infant Formula Powder by Ion Chromatography Coupled with Tandem Mass Spectrometry Based on Captiva EMR-Lipid Clean-up [J]. FOOD SCIENCE, 2021, 42(12): 315-321.
[2]	WANG Yan, WANG Juan, WU Chunmin, ZHANG Chunlin, WANG Dong, GAO Zhuo, ZHANG Leilei, ZHANG Yan. Determination of Inositol in Infant Formula and Milk by Ion Chromatography-Tandem Triple Quadrupole Mass Spectrometry [J]. FOOD SCIENCE, 2020, 41(24): 185-189.
[3]	JI Fengdi, XIA Rong, TAO Huiyuan, WEI Wei, MU Xiaoting, LI Dong, LU Fei. Determination of Organic Acids in Vinegar and Related Products by Ion Chromatography [J]. FOOD SCIENCE, 2020, 41(18): 239-244.
[4]	SHENG Huadong, PAN Xiangjie, ZHANG Shuifeng, LIU Minfang, SHI Yuanxu, WANG Lulu, LU Wenqi. Simultaneous Determination of Perchlorate, Chlorate and Bromate in Vegetables and Fruits by Modified QuEChERS Method Coupled with UPLC-MS/MS [J]. FOOD SCIENCE, 2020, 41(10): 324-329.
[5]	CHEN Huiling, SHEN Jinshan, WANG Xueguang, YANG Lixin. Dietary Pollution Status and Exposure Risk Assessment of Short-Chain Chlorinated Paraffins [J]. FOOD SCIENCE, 2019, 40(21): 143-149.
[6]	YANG Jinquan, HE Xiaomin, SHI Minfang, CHEN Hao, LI Yongrong, ZHU Youlin. YANG Jinquan, HE Xiaomin, SHI Minfang, CHEN Hao, LI Yongrong, ZHU Youlin [J]. FOOD SCIENCE, 2019, 40(20): 332-337.
[7]	XIE Pujun, HUANG Lixin, ZHANG Caihong, DING Shasha, DENG Yejun, WANG Xiaojie. Characterization, Antioxidant Activity and Thermostabiltiy of Hydroxytyrosol Polymerization Products Catalyzed by Laccase [J]. FOOD SCIENCE, 2018, 39(16): 90-97.
[8]	HUANG Shuangxia, HOU Dianzhi, CHEN Hualei, YU Yue, CHEN Shan,. Determination of Dextransucrase-Catalyzed Reaction Products of Sucrose by High Performance Gel Filtration Chromatography with Tandem Two Columns and Analysis of the Dextran Polymerization Process [J]. FOOD SCIENCE, 2018, 39(12): 191-198.
[9]	ZHU Wei, NING Xiaojun, DU Ruyun. Determination of Functional Oligosaccharides in Infant Formula Milk Powder by High Performance Ion Chromatography [J]. FOOD SCIENCE, 2017, 38(24): 224-228.
[10]	LI Rong, YU Jun, JIANG Zitao, HUANG Xianyong. Preparation of Umami Peptide by Microwave-Assisted Stepwise Enzymatic Hydrolysis of Perilla Seed Meal Protein [J]. FOOD SCIENCE, 2017, 38(20): 169-175.
[11]	YE Mei, WU Wenlin, GUO Liang, XIAO Quanwei, LIANG Hengxing, WAN Yuping. Rapid Determination of Cyanide in Mixed Wines by Ion Chromatography with Pulsed Amperometric Detection [J]. FOOD SCIENCE, 2016, 37(8): 192-195.
[12]	DUAN Bing, HE Taixi, FAN Yuanyuan, ZHENG Bing. Determination of Imidacloprid and Acetamiprid in Tea by Gel Permeation ChromatographyUltra Performance Liquid Chromatography-Tandem Mass Spectrometry [J]. FOOD SCIENCE, 2016, 37(4): 238-241.
[13]	Lü Zhenzhen, JIAO Zhonggao, LIU Jiechao, LIU Hui, ZHANG Chunling, YANG Wenbo. Response Surface Optimization of Ultrasonic-Assisted Extraction and HPCPC Purification of Amygdalin from Bitter Apricot Kernel Meal (Prunus armeniaca) [J]. FOOD SCIENCE, 2016, 37(24): 74-80.
[14]	XU Meng, LIU Wei, ZHOU Li, MA Zhifang, PENG Zengqi. Ion Chromatography Studies of Dynamic Hydrolysis of Added Polyphosphates in Muscle [J]. FOOD SCIENCE, 2016, 37(19): 36-41.
[15]	LI Wenjie, LI Hongfei, WANG Weihao, JIA Pengyu, KANG Lijun, KOU Fang, ZHANG Lili, YIN Jing, CAO Longkui. Optimization of Microwave/Ultrasonic-Assisted Sulfuric Acid Hydrolysis of Corn Straw by Using Response Surface Methodology [J]. FOOD SCIENCE, 2016, 37(14): 43-50.

Simultaneous Determination of Bromate, Chlorite, Chlorate and Common Inorganic Anions in Drinking Water by Ion Chromatography

RichHTML

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments