FOOD SCIENCE ›› 2001, Vol. 22 ›› Issue (11): 73-75.

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Determination of Organochlorine Pesticide Residues in Tea by CGC-ECD

 HAO  Gui-Ming,   Li-Huan-Xin,   Zhao-Chun-Jie,   E-Yun-Juan   

  • Online:2001-11-15 Published:2012-02-14

Abstract: Objective To determine 12 organochlorine pesticide residues in Tea by capillary gas chromatography with electron capture detector (CGC- ECD). Method Samples were extracted by FDA method. The capillary column was DB- 1(30m× 0.25mm × 0.25μ m);injector temperature was 250℃ and detector temperature was 280℃ ;The column temperature program was initial temperature 150℃ with rate of 15℃ /min to 180℃ (hold 1min), rate of 10℃ /min to 210℃ (hold 2min),and rate of 15℃ /min to 240℃ (hold 10min). The pesticide residues were calculated by external standard method. Results the average recoveries and RSD ranged from 80.1% to 103.8% and 0.52% to 6.21% respectively, at three spiked mixed organochlorine pesticide levels. All the samples showed organochlorine pesticide residues. Conglusion The method is easy in operation and has good separation and repeatability.

Key words:  , Tea Organochlorine pesticide residues Capillary gas chromatography;