食品科学 ›› 2009, Vol. 30 ›› Issue (18 ): 209-211.doi: 10.7506/spkx1002-6300-200918044

• 工艺技术 • 上一篇    下一篇

陶瓷膜在D- 异抗坏血酸钠精制中的应用

魏 转1,王亚坤2,孙文敬2 , 3 ,*,崔文元4,孙祎敏1,王 萍1   

  1. 1.河北化工医药职业技术学院制药工程系 2.河北师范大学生命科学学院 3.江苏大学食品与生物工程学院 4.河北师范大学物理学院
  • 收稿日期:2009-06-12 出版日期:2009-09-15 发布日期:2010-12-29
  • 通讯作者: 孙文敬 E-mail:sunwenjing1919@163.com
  • 基金资助:

    江西省主要学科学术和技术带头人培养计划项目(2008DD00600)

Application of Ceramic Membrane Filtration in Purification of Sodium Erythorbate

WEI Zhuan1,WANG Ya-kun2,SUN Wen-jing2,3,*,CUI Wen-yuan4,SUN Yi-min1,WANG Ping1   

  1. 1. Department of Pharmaceutical, Hebei Chemical and Pharmaceutical College, Shijiazhuang 050026, China;
    2. College of Life Science, Hebei Normal University, Shijiazhuang 050016, China;
    3. College of Food and Biological Engineering, Jiangsu University, Zhenjiang 212013, China;
    4. College of Physics, Hebei Normal University, Shijiazhuang 050016, China
  • Received:2009-06-12 Online:2009-09-15 Published:2010-12-29
  • Contact: SUN Wen-jing E-mail:sunwenjing1919@163.com

摘要:

初步考察D- 异抗坏血酸钠精制过程中滤材对产品质量的影响。结果表明,在过滤D- 异抗坏血酸钠粗品溶液中的活性炭时,采用陶瓷膜代替滤布作为滤材,能够有效地改善产品质量,并有助于精制收率的提高。在压力0.15MPa、温度80℃、表面流速2m/s 和浓缩15 倍条件下,陶瓷膜的平均通量高达490L/(m2·h)左右;在膜通量350~390L/(m2·h)时,其余条件同上;浓缩倍数可达20 倍,能够满足工业生产的要求。

关键词: D- 异抗坏血酸钠, 陶瓷膜, 精制

Abstract:

The effects of various filtration materials used in the purification of sodium erythorbate on product quality were investigated. The results indicated that when ceramic membrane was used for the filtration of active carbon in crude product solution instead of filtration cloth, the product quality was significantly improved, and the purification yield was increase at the same time. Under the following operation conditions: pressure 0.15 MPa, temperature 80 ℃, surface flow rate 2 m/s, and concentration fold 15, the average membrane flux was as high as 490 L/(m2·h). When the membrane flux ranged from 350 to 390 L/(m2 ·h) and other conditions were the same as above, a 20-fold concentration was obtained, which could fulfill the need of industrial production of sodium erythorbate.

Key words: sodium erythorbate, ceramic membrane, purification

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