食品科学 ›› 2010, Vol. 31 ›› Issue (12): 144-147.doi: 10.7506/spkx1002-6630-201012033

• 工艺技术 • 上一篇    下一篇

固体酸水解法制备牛蒡果糖工艺的研究

王 磊,马利华* ,秦卫东,陈学红,张 旭   

  1. 徐州工程学院食品学院
  • 收稿日期:2009-09-21 修回日期:2010-02-02 出版日期:2010-06-15 发布日期:2010-12-29
  • 通讯作者: 马利华 E-mail:mlh6610@163.com

Solid Acid-catalyzed Hydrolysis of Burdock Roots for Fructose Preparation

WANG Lei,MA Li-hua*,QIN Wei-dong,CHEN Xue-hong,ZHANG Xu   

  1. College of Food Engineering, Xuzhou Institute of Technology, Xuzhou 221008, China
  • Received:2009-09-21 Revised:2010-02-02 Online:2010-06-15 Published:2010-12-29
  • Contact: MA Li-hua*, E-mail:mlh6610@163.com

摘要:

以牛蒡为原料,对以强酸型阳离子交换树脂D061为固体酸水解牛蒡制备果糖的工艺进行研究。考察固体酸与牛蒡浸提液的体积比、水解温度、水解时间、固体酸重复使用次数4 个影响制备果糖工艺条件的主要因素。结果表明:固体酸法可以水解牛蒡制备出高质量的果糖,最佳水解工艺条件为水解时间120min、水解温度75℃、固体酸与牛蒡浸提液的体积比为1:2,重复使用固体酸水解3 次后,水解率为76.7%,还原糖含量为145.8g/L。

关键词: 牛蒡, 水解, 固体酸, 果糖

Abstract:

Burdock roots containing inulin provided a raw material for the preparation of fructose derived from hydrolyzed inulin. D061 strong cation resin, a solid acid was used as catalyzer to prepare fructose. The effects of the main hydrolysis conditions, i.e., solid-to-liquid ratio, hydrolysis temperature, length of hydrolysis time and hydrolysis times on hydrolysis rate and reducing sugar content were investigated by single factor and orthogonal array design methods. The results showed that the use of D061 strong cation resin to repeatedly extract the material 3 times at 75 ℃ and 1:2 solid-to-liquid ratio for 120 min each time provided an optimal hydrolysis, and the resulting hydrolysis rate and reducing sugar content were 76.7% and 145.8 g/L, respectively.

Key words: burdock, hydrolysis, solid acid, fructose

中图分类号: