食品科学 ›› 2007, Vol. 28 ›› Issue (10): 165-167.

• 工艺技术 • 上一篇    下一篇

红枣中齐墩果酸提取工艺的研究

 曹艳萍, 杨秀利, 薛成虎   

  1. 榆林学院化学系; 济南大学化学化工学院; 榆林学院化学系 陕西榆林719000; 山东济南250022; 陕西榆林719000;
  • 出版日期:2007-10-15 发布日期:2011-11-22

Study on Extraction Technology of Oleanolic Acid in Zizyphus jujuba Date

 CAO  Yan-Ping, YANG  Xiu-Li, XUE  Cheng-Hu   

  1. 1.Department of Chemistry, Yulin College, Yulin 719000, China; 2.College of Chemical Technology, Ji’nan University, Jinan 250022, China
  • Online:2007-10-15 Published:2011-11-22

摘要: 对红枣中齐墩果酸的95%乙醇提取工艺进行了研究。用HPLC法测定齐墩果酸含量,通过L9(34)正交试验,优选了工业参数。结果表明:对提取效果影响因素依次为浸提温度>浸提时间>料液比>粒度。最佳提取工艺条件是:浸提温度70℃,浸提时间3h,料液比1:20,原料粒度100目。提取率为1.581g/kg。

关键词:  , 红枣, 齐墩果酸, 提取, 工艺

Abstract: The extraction technology of oleanolic acid in Zizyphus jujuba mill was studied with ethanol as extractor. The contained amount of quercitr was assayed by HPLC. The best conditions were chosen through L9(34) orthogonal test. The results showed the first factor affecting extraction rate was volume percentage of ethonal, and the second and the third ones were temperature and rotio of feed liqued respectively. The best extraction conditions were 70% ethanol as extractant with the granularity of 100 mesh at the temperature of 50 ℃ for 3 h. The extraction rate was 1.549 g/kg.

Key words: Zizyphus jujuba dates, oleanolic acid, extraction, technology