食品科学 ›› 2019, Vol. 40 ›› Issue (12): 78-84.doi: 10.7506/spkx1002-6630-20181028-321

• 食品化学 • 上一篇    下一篇

虫白蜡高级烷醇微乳液的制备及其在功能饮料中的应用

马金菊1,马李一1,李 凯1,张雯雯1,张玉荣2,杨茂栋3,陈晓鸣1,张 弘1,*   

  1. 1.中国林业科学研究院资源昆虫研究所,国家林业局特色森林资源工程技术研究中心,云南 昆明 650224;2.湖南省林业科学院,湖南 长沙 410000;3.芷江县华耘虫白蜡有限责任公司,湖南 芷江 419100
  • 出版日期:2019-06-25 发布日期:2019-06-28
  • 基金资助:
    中央级公益性科研院所基本科研业务费专项(CAFYBB2018SY025)

Preparation of Microemulsion with Policosanol Derived from Insect Wax and Its Application in Functional Beverage

MA Jinju1, MA Liyi1, LI Kai1, ZHANG Wenwen1, ZHANG Yurong2, YANG Maodong3, CHEN Xiaoming1, ZHANG Hong1,*   

  1. 1. Research Center of Engineering and Technology on Forest Resources with Characteristics, State Forestry Administration, Research Institute of Resources Insects, Chinese Academy of Forestry, Kunming 650224, China; 2. Hunan Academy of Forestry, Changsha 410000, China; 3. Zhijiang Huayun Insect Wax Co. Ltd., Zhijiang 419100, China
  • Online:2019-06-25 Published:2019-06-28

摘要: 为解决虫白蜡高级烷醇不溶于水,难应用于澄清稳定型功能饮料的瓶颈问题,制备高负载量的高级烷醇微乳液,获得其最佳乳化条件,通过伪三元相图确定微乳区域,评价其稳定性,并将其作为功能性添加剂配制高级烷醇功能饮料。结果表明:当复配乳化剂亲水亲油平衡值为10,乳化温度为70~75 ℃时,得到各添加剂用量均在食品国家标准允许添加范围内的稳定澄清的高级烷醇微乳液;微乳的离心、冷热循环和稀释稳定性良好,室温贮藏65 d后依然稳定透明;伪三元相图中微乳区域随着Km值的减小而不断缩小;微乳与其他辅料复配后可以制备成透明稳定的高级烷醇功能饮料。将虫白蜡高级烷醇制备成微乳,有效解决了其不溶于水以及在饮料中稳定性差、极易上浮等问题,为制备高品质、透明稳定的高级烷醇功能饮料提供了一条有效途径,也为高级烷醇新产品的开发研究提供参考。

关键词: 高级烷醇, 微乳液, 伪三元相图, 功能饮料

Abstract: The poor water solubility of policosanol hinders it from being applied in clear and stable functional beverages. To solve this bottleneck problem, a microemulsion with high loading of policosanol was prepared in this study. The optimum emulsification conditions were obtained. The microemulsion area was determined by constructing a pseudo-ternary-phase diagram and the stability was evaluated. The microemulsion was used as a functional ingredient in beverage. The results indicated that the microemulsion, prepared with an emulsifier mixture with a hydrophile-lipophile balance (HLB) value of 10 at emulsifying temperatures of 70–75 ℃, was stable and transparent, in which the amount of each additive was within the limits of the national standards for food safety. The microemulsion was stable against centrifugation, alternating hot and cold cycles and dilution. It was stable and transparent for 65 days at room temperature. With the decrease of the Km value, the microemulsion area in the pseudo-ternary-phase diagram decreased. A stable and transparent functional beverage was prepared based on the policosanol-loading microemulsion. The microemulsification of policosanol effectively improved its poor water solubility and stability in beverage, which provides a valid way of preparing high quality, transparent and stable functional beverage containing policosanol and lays the foundation for the development of new products.

Key words: policosanol, microemulsion, pseudo-ternary phase diagram, functional beverage

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