食品科学 ›› 2009, Vol. 30 ›› Issue (12): 215-218.doi: 10.7506/spkx1002-6630-200912048

• 分析检测 • 上一篇    下一篇

自动化静态顶空/气相色谱-质谱对胶州大白菜中风味物质的快速分析

吴 澎1,周 涛2,寇丽娟1,王 超2   

  1. 1.山东农业大学食品科学与工程学院 2. 山东农业大学园艺科学与工程学院
  • 收稿日期:2008-09-16 修回日期:2009-01-05 出版日期:2009-06-15 发布日期:2010-12-29
  • 通讯作者: 吴澎 E-mail:wupengguai@163.com
  • 基金资助:

    作物生物学国家重点实验室开放课题(200707)

Automatic Static Headspace GC-MS Analysis of Flavor Compounds in Two Jiaozhou Chinese Cabbage Varieties and Tai'an Chinese Cabbage

WU Peng1,ZHOU Tao2,KOU Li-juan1,WANG Chao2   

  1. (1. College of Food Science and Engineering, Shandong Agricultural University, Tai'an 271018, China;
    2. College of Horticulture Science and Engineering, Shandong Agricultural University, Tai 'an 271018, China)
  • Received:2008-09-16 Revised:2009-01-05 Online:2009-06-15 Published:2010-12-29
  • Contact: WU Peng1, E-mail:wupengguai@163.com

摘要:

采用静态顶空和气质联用的方来来分析对比“胶白”与泰安当地产普通大白菜的挥发性成分,通过GCMS分析和NIST 质谱谱库计算机检索,对样品进行定性分析,并采用面积归一化法进行定量分析。结果表明:十八烯酸(Z)- 甲酯和十六烷酸- 甲酯是对胶白风味起决定作用的物质,静态顶空- 气相色谱- 质谱分析是一种快速有效分析蔬菜中风味物质成分的方法。

关键词: 静态顶空- 气相色谱- 质谱分析, 风味物质, 胶州大白菜, 泰安大白菜

Abstract:

A method using automatic static headspace GC-MS was developed for the determination of flavor compounds in Chinese cabbages. The qualitative and quantitative analysis was performed by search program of NIST mass spectral library and area normalization method, respectively. The flavor compounds in two Jiaozhou Chinese cabbage varieties (Jiaozhou No. 3 and Hongshengbai) and Taian Chinese cabbage were compared. Results indicated that 9,12-octadecadienoic acid (Z,Z)-, methyl ester and 9-octadecenoic acid (Z)-, methyl ester were the main compounds attributing to the flavor of Jiaozhou Chinese cabbage, while they were not detected in Taian Chinese cabbage. This method is proved to be fast and reliable for analyzing the flavor compounds in vegetables.

Key words: automatic static headspace GC-MS, flavor compounds, Jiaozhou Chinese cabbage, Tai'an Chinese cabbage

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