食品科学 ›› 1997, Vol. 18 ›› Issue (9): 51-55.

• 食品科学 • 上一篇    下一篇

折光率检测器离子交换HPLC法测定葡萄酒和葡萄汁中主要有机酸、糖、甘油和乙醇

 张学俊   

  1.  温州大学
  • 出版日期:1997-09-15 发布日期:2011-12-16

   Zhang-Xue-Jun   

  • Online:1997-09-15 Published:2011-12-16

摘要:  提出一个利用折光率检测器、离子交换、HPIC同时分离和测定葡萄酒和葡萄汁中主要有机酸、糖、甘油和乙醇的方法。用一个强阴离子交换的固相萃取柱消除糖对酸测定的干扰,从而实现对甜葡萄酒和葡萄汁中苹果酸的准确测定,并对该法的线性范围、相关系数、标准偏差、以及不同方法进行了的分析对比。

关键词: 高效液相色谱, 葡萄酒分析, 折光率检测器

Abstract: The method to determin the major Carboxylic acids, Sugars, glucerol and ethanol in wine and grape must is developled using an ion-exchange column and refractive index detector. A solid-phase extraction method with a strong anion exchanger is used to determine these compounds. The method is validated by determining the repeatability, reproducibility, correlation coefficients, recovery efficienty and accuracy and was compared with different methods of analysis.

Key words: High-performance liquid chromatography Analysis of wine Refractive index detector