Response Surface Methodology as An Approach to Optimization of Synthesis of Soybean Sucrose Polyester

doi:10.7506/spkx1002-6300-201008003

FOOD SCIENCE ›› 2010, Vol. 31 ›› Issue (8): 11-15.doi: 10.7506/spkx1002-6300-201008003

• Processing Technology • Previous Articles Next Articles

Response Surface Methodology as An Approach to Optimization of Synthesis of Soybean Sucrose Polyester

WANG Li-bin1,2，LI Wen-lin1，ZHANG Qiang3，HUANG Feng-hong1,*

1. Institute of Oil Crops Research, Chinese Academy of Agricultural Sciences, Wuhan 430062, China；
2. College of Food Science and Technology, Huazhong Agricultural University, Wuhan 430070, China；
3. Center Laboratory of Tianjin Academy of Agricultural Sciences, Tianjin 300381, China)

Received:2009-07-15 Revised:2009-11-27 Online:2010-04-15 Published:2010-12-29
Contact: HUANG Feng-hong1 E-mail:huangfh@oilcrops.cn

Abstract

Abstract:

Cetyltrim ethylammonium bromide was used as phase-transfer catalyst to synthesize soybean sucrose polyester from ethyl-esterfied soybean oil and sucrose by two-step method. Response surface analysis based on Box-Behnken experimental design was used to investigate the optimal values of reaction temperature, catalyst amount, ethyl-esterfied soybean oil/sucrose molar ratio and reaction time affecting soybean sucrose polyester yield. Results showed that under the following optimized conditions: reaction temperature 135.6 ℃, catalyst amount 4.1%, ethyl-esterfied soybean oil/sucrose molar ratio 13.5:1 and reaction time 5.5 h, the soybean sucrose polyester yield and the esterfication degree were up to 90.72% and 7.1, respectively.

Key words: sucrose, ethyl ester, soybean oil sucrose polyester, phase-transfer catalyst, response surface methodology

CLC Number:

TS225.13

WANG Li-bin1,2，LI Wen-lin1，ZHANG Qiang3，HUANG Feng-hong1,*. Response Surface Methodology as An Approach to Optimization of Synthesis of Soybean Sucrose Polyester[J]. FOOD SCIENCE, 2010, 31(8): 11-15.

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Response Surface Methodology as An Approach to Optimization of Synthesis of Soybean Sucrose Polyester

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