Determination of Diethylstilbestrol Residue in Aquatic Products by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

doi:10.7506/spkx1002-6630-200908044

FOOD SCIENCE ›› 2009, Vol. 30 ›› Issue (8): 207-208.doi: 10.7506/spkx1002-6630-200908044

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Determination of Diethylstilbestrol Residue in Aquatic Products by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

XU Ying-jiang GONG Xiang-hong ZHANG Xiu-zhen

(Research Institute of Marine Fisheries of Shandong Province, Yantai 264006, China)

Received:2008-05-27 Revised:2008-06-30 Online:2009-04-15 Published:2010-12-29
Contact: XU Ying-jiang E-mail:xu_ying_jiang@sina.com

Abstract

Abstract:

The method for determination of diethylstilbestrol (DES) residues in aquatic products by UPLC-MS/MS was developed. The DES residues were extracted with ethyl acetate, purified with SLH solid phase extraction cartridge, determined by UPLC-MS/MS and quantified by external standard method. When adding diethylstilbestrol to samples in a range of 0.1 to 1.0 μg/kg, the recoveries are above 75%, the relative standard deviations are between 5.5% and 9.2%.

Key words: UPLC-MS/MS, diethylstilbestrol, aquatic products

CLC Number:

TS207.5

XU Ying-jiang GONG Xiang-hong ZHANG Xiu-zhen. Determination of Diethylstilbestrol Residue in Aquatic Products by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry[J]. FOOD SCIENCE, 2009, 30(8): 207-208.

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Determination of Diethylstilbestrol Residue in Aquatic Products by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

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